Study on Soil Pretreatment Methods of Tetracycline Antibiotics
In order to establish a pre-treatment method for the determination of tetracycline antibiot-ics in soil,including shaking extraction,freezing separation,and small column purification,the pre-treatment techniques of three tetracycline antibiotics in soil,including extraction methods,extrac-tion solvent types,purification methods,and preservation conditions of the extraction solution,were studied.The tetracycline antibiotics were determined using a liquid chromatography tandem mass spectrometer.The recovery rates of tetracycline antibiotics at different concentration levels using this method range from 80.0%to 118.0%,with a relative standard deviation of less than 20%.This pre-treatment method has strong adaptability,simple operation,and high extraction efficiency,making it suitable for the analysis of tetracycline antibiotic residues in soil.
tetracyclinesvibrating extractionfreezing separationliquid chromatography tandem mass spectrometer
国家科技期刊平台
NSTL
万方数据
维普
