石煤钒矿低温硫酸熟化-水浸提钒工艺
Low Temperature Sulfuric Acid Ripening-water Leaching for Vanadium Extraction from Stone Coal Vanadium Ore
曹欢 1靳建平 1赵笑益 1梁效 1宁新霞1
作者信息
- 1. 西安西北有色地质研究院有限公司,陕西省矿产资源综合利用工程技术研究中心,陕西 西安 710054
- 折叠
摘要
这是一篇冶金工程领域的论文.以陕西某地含钒矿物为绢云母、伊利石的石煤钒矿为研究对象,采用低温硫酸熟化-水浸工艺提钒,考查了熟化温度、熟化时间、硫酸用量、氯化钠用量,浸出温度、浸出时间及浸出液固比对钒浸出率的影响.结果表明:向石煤钒矿中加入25%的硫酸、0.8%的氯化钠,在130 ℃下熟化8h,熟化样品在浸出温度55 ℃、液固比1.5∶1的条件下浸出时间2h,钒浸出率可达89%.这说明采用低温(130℃)硫酸熟化-水浸工艺提取石煤型钒矿是可行的.
Abstract
This is an article in the field of metallurgical engineering.The vanadium ore with vanadium containing sericite and illite in Shaanxi province was taken as the research object,low-temperature sulfuric acid ripening-water leaching process was used to extract vanadium.The effects of ripening temperature,ripening time,sulfuric acid dosage,sodium chloride dosage,leaching temperature,leaching time and liquid-solid ratio on vanadium leaching rate were investigated.The results show when 25%sulfuric acid and 0.8%sodium chloride are added to the stone coal vanadium ore,the sample is aged at 130 ℃ for 8 h,and the sample is leached at 55 ℃ for 2 h under the conditions of liquid-solid ratio of 1.5∶1,the vanadium leaching rate can reach more than 89%.This indicates that it is feasible to adopt low temperature sulfuric acid ripening and water leaching process to extract stone coal type vanadium ore.
关键词
冶金工程/石煤钒矿/硫酸熟化/提钒/水浸Key words
Metallurgical engineering/Stone coal vanadium ore/Sulfuric acid ripening/Extracting vanadium/Water leaching引用本文复制引用
基金项目
陕西省创新人才推进计划(2020KJXX-053)
出版年
2024