矿产综合利用2024,Vol.45Issue(3) :75-80.DOI:10.3969/j.issn.1000-6532.2024.03.012

石煤钒矿低温硫酸熟化-水浸提钒工艺

Low Temperature Sulfuric Acid Ripening-water Leaching for Vanadium Extraction from Stone Coal Vanadium Ore

曹欢 靳建平 赵笑益 梁效 宁新霞
矿产综合利用2024,Vol.45Issue(3) :75-80.DOI:10.3969/j.issn.1000-6532.2024.03.012

石煤钒矿低温硫酸熟化-水浸提钒工艺

Low Temperature Sulfuric Acid Ripening-water Leaching for Vanadium Extraction from Stone Coal Vanadium Ore

曹欢 1靳建平 1赵笑益 1梁效 1宁新霞1
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作者信息

  • 1. 西安西北有色地质研究院有限公司,陕西省矿产资源综合利用工程技术研究中心,陕西 西安 710054
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摘要

这是一篇冶金工程领域的论文.以陕西某地含钒矿物为绢云母、伊利石的石煤钒矿为研究对象,采用低温硫酸熟化-水浸工艺提钒,考查了熟化温度、熟化时间、硫酸用量、氯化钠用量,浸出温度、浸出时间及浸出液固比对钒浸出率的影响.结果表明:向石煤钒矿中加入25%的硫酸、0.8%的氯化钠,在130 ℃下熟化8h,熟化样品在浸出温度55 ℃、液固比1.5∶1的条件下浸出时间2h,钒浸出率可达89%.这说明采用低温(130℃)硫酸熟化-水浸工艺提取石煤型钒矿是可行的.

Abstract

This is an article in the field of metallurgical engineering.The vanadium ore with vanadium containing sericite and illite in Shaanxi province was taken as the research object,low-temperature sulfuric acid ripening-water leaching process was used to extract vanadium.The effects of ripening temperature,ripening time,sulfuric acid dosage,sodium chloride dosage,leaching temperature,leaching time and liquid-solid ratio on vanadium leaching rate were investigated.The results show when 25%sulfuric acid and 0.8%sodium chloride are added to the stone coal vanadium ore,the sample is aged at 130 ℃ for 8 h,and the sample is leached at 55 ℃ for 2 h under the conditions of liquid-solid ratio of 1.5∶1,the vanadium leaching rate can reach more than 89%.This indicates that it is feasible to adopt low temperature sulfuric acid ripening and water leaching process to extract stone coal type vanadium ore.

关键词

冶金工程/石煤钒矿/硫酸熟化/提钒/水浸

Key words

Metallurgical engineering/Stone coal vanadium ore/Sulfuric acid ripening/Extracting vanadium/Water leaching

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基金项目

陕西省创新人才推进计划(2020KJXX-053)

出版年

2024
矿产综合利用
中国地质科学院矿产综合利用研究所

矿产综合利用

CSTPCD
影响因子:0.643
ISSN:1000-6532
参考文献量15
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