By comparing and analyzing the four control indicators of gas phase content,liquid phase content,chromaticity,and acid value of TAIC products obtained from experiments,the optimal raw material ratio and reaction conditions with a yield of over 90％were determined.The mass ratio of raw materials was m(trisodium isocyanurate)∶m(allyl chloride)∶m(catalyzer)∶m(dehydrating agent)∶m(solvent)=100∶130∶2.4∶1∶300.The reaction temperature was controlled at 95 ℃.
关键词
三烯丙基异氰脲酸酯/异氰尿酸三钠/氯丙烯/反应温度/原料配比/色度/酸值/收率
Key words
triallyl isocyanurate/trisodium isocyanurate/allyl chloride/reaction temperature/raw material ratio/chrominance/acid value/yield
维普
万方数据