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固相微萃取一气相色谱质谱法测定水中异味物质实验

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利用固相微萃取(SPME)结合气相色谱—质谱(GC-MS)技术,对水体中异味物质进行了定性与定量分析。针对水体异味对环境和居民生活造成的严重影响,综述了国内外在异味物质检测领域的研究现状,并详细阐述了实验过程。通过优化固相微萃取的多个条件,包括涂层选择、氯化钠加入量、萃取时间、萃取温度、振荡速度及脱附时间,确定最佳实验参数。实验结果表明:该方法具有良好的线性关系和较低的检出限,能够准确、灵敏地检测水体中的异味物质。通过实际样品分析,验证了该方法的可行性和有效性,为水中异味物质的监测与治理提供了科学依据。
Determination of Odorous Substances in Water by Solid Phase Microextraction and Gas Chromatography-Mass Spectrometry
In this paper,Solid Phase Microextraction(SPME)combined with Gas Chromatography-Mass Spec-trometry(GC-MS)was used for qualitative and quantitative analysis of odorous substances in water.In view of the serious impact of water odor on the environment and residents'life,the research status of odor detection at home and abroad was reviewed,and the experimental process was described in detail.The optimum experimental param-eters were determined by optimizing several conditions of SPE,including coating selection,sodium chloride addi-tion,extraction time,extraction temperature,oscillation speed and desorption time.The experimental results show that the method has good linear relationship and low detection limit,and can accurately and sensitively detect odorous substances in water.Finally,the feasibility and effectiveness of the method were verified by actual sample analysis,which provided a scientific basis for the monitoring and control of odorous substances in water.

solid phase microextractionGas Chromatograph-Mass Spectrometry(GC-MS)odorous substances in waterdetection method

张建勋

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苏州市吴江环境监测站,江苏 苏州 215200

固相微萃取 气相色谱—质谱(GC-MS) 水中异味物质 检测方法

2024

绿色科技
花木盆景杂志社

绿色科技

影响因子:0.365
ISSN:1674-9944
年,卷(期):2024.26(22)