首页|多级孔MOFs材料结合HPLC法同时检测肉制品中4种偶氮类合成着色剂

多级孔MOFs材料结合HPLC法同时检测肉制品中4种偶氮类合成着色剂

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以多级孔 MOFs材料(macro-microporous ZIF-8,M-ZIF-8)作为吸附剂进行净化,建立高效液相色谱法(HPLC)同时检测肉制品中4种偶氮类合成着色剂(胭脂红、日落黄、柠檬黄、苋菜红)的方法.结果表明:在优化仪器条件下,4种偶氮类合成着色剂线性良好,相关系数大于0.999,定量限(LOQs)为0.3~0.5 mg/kg,回收率为92.0%~105.1%,相对标准偏差为0.5%~2.2%.该方法高效快捷,可以同时检测肉制品中的4种偶氮类合成着色剂,缩短了前处理时间,且可循环使用至少5次,降低分析成本.因此,该方法在肉制品中偶氮类合成着色剂的检测中具有较好的运用前景.
Simultaneous detection of four azo synthetic colorants in meat products using multi-stage porous MOFs materials combined with high-performance liquid chromatography
A high-performance liquid chromatography(HPLC)method was established for the simultaneous detection of four azo synthetic colorants(carmine,sunset yellow,lemon yellow,amaranth)in meat products,using multi porous MOFs(macro microporous ZIF-8,M-ZIF-8)as adsorbents for purification.The results showed that under optimized instrument conditions,the four azo based synthetic colorants had good linearity,with a correlation coeffi-cient greater than 0.999,a limit of quantification(LOQs)of 0.3-0.5 mg/kg,a recovery rate of 92.0%-105.1%,and a relative standard deviation of 0.5%-2.2%.This method is efficient and fast,capable of simultaneously detecting four types of azo synthetic colorants in meat prod-ucts,shortening the pre-treatment time,and can be reused at least 5 times,reducing analysis costs.Therefore,this method has good application prospects in the detection of azo synthetic col-orants in meat products.

macro-microporous ZIF-8high performance liquid chromatography(HPLC)ad-sorbentmeat productsazo synthetic colorants

陈丹丹、陈彬、胡雨、管彬彬、丁红梅

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南通市食品药品监督检验中心(南通 226014)

多级孔MOFs 高效液相色谱法(HPLC) 吸附剂 肉制品 偶氮类合成着色剂

2025

粮食与食品工业
国家粮食储备局无锡科研设计院 中国粮油学会

粮食与食品工业

影响因子:0.503
ISSN:1672-5026
年,卷(期):2025.32(1)