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煤层水中甲醛含量的快速检测方法研究

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研究了采用乙酰丙酮分光光度法测定煤层水中甲醛的方法,并对检出限、精密度和准确度进行了方法验证.结果表明:甲醛检出限为 0.012 98 mg/L;对 3 种浓度的甲醛标准使用溶液样品进行测试,相对标准偏差分别为 1.54%、0.377 3%、0.168 7%;样品加标回收率在 101.01%~103.33%;以上各项指标均满足HJ 601-2011 方法要求,说明采用分光光度法可以快速准确测定煤层水中甲醛的含量.
Research on rapid detection method for formaldehyde content in coal seam water
The method of using acetylacetone spectrophotometry to determine formaldehyde in coal seam water was studied,and the detection limit,precision and degree of accuracy were validated.The results showed that the detection limit of formaldehyde was 0.012 98 mg/L.And three concentrations of formaldehyde standard solution samples were tested with relative standard deviations of 1.54%,0.377 3%and 0.168 7%respectively.The recovery rate of sample spiking was between 101.01%and 103.33%.All the above indicators met the requirements of HJ 601-2011,indicating that the use of spectrophotometry could quickly and accurately determine the content of formaldehyde in coal seam water.

coal seam waterformaldehydespectrophotometerdetection limitprecisiondegree of accuracy

吴鹏、宋燕莉、刘健

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煤与煤层气共采国家重点实验室,山西 晋城 048000

易安蓝焰煤与煤层气共采技术有限责任公司,山西 晋城 048000

煤层水 甲醛 分光光度计 检出限 精密度 准确度

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20191102001

2024

煤化工
赛鼎工程有限公司(原中国化学工业第二设计院),全国煤化工信息站,全国煤化工设计技术中心

煤化工

CSTPCD
影响因子:0.629
ISSN:1005-9598
年,卷(期):2024.52(1)
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