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水煤浆气化粗渣制备泡沫材料及其吸波性能研究

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水煤浆气化粗渣颗粒经过高温焙烧后出现发泡黏结现象,为利用其制备泡沫材料提供了基础。以宁东四喷嘴水煤浆气化粗渣为原料,采用单一变量法依次探究了粗渣用量、焙烧温度、保温时间对泡沫材料抗压强度和体积密度的影响。结果表明,在粗渣粒度为1。25~5 mm,粗渣用量为14 g(固定容积的模具),焙烧气氛为N2,焙烧温度为 750℃,保温时间为 10 min的条件下,制备出的泡沫材料的抗压强度高于1。5 MPa,体积密度低于 0。5 g/cm3。该材料的电磁波吸收性能为:当材料厚度为7 mm时,最低反射损耗值为-22。14 dB(16。80 GHz),有效带宽为1。88 GHz。它对电磁波的吸收主要体现在16~18 GHz频段,吸收损耗机制以气化渣中丰富铁氧体的磁损耗作用为主。可为水煤浆气化粗渣在泡沫材料的制备及其在吸波领域的应用提供新的思路。
Foam materials preparation of coarse slag from coal-water slurry gasification and its absorption properties
The foaming and bonding phenomenon occurs in the coarse slag particles of coal water slurry gasification after high temperature roasting,which provides a basis for the preparation of foam materials.Single variable method is used to explore the effects of slag amount,roasting temperature and holding time on the compressive strength and volume density of foam materials,using Ningdong four nozzle coal water slurry gasification slag as raw material.The results show that,under the conditions of 1.25~5 mm coarse slag particle size,14 g coarse slag amount(fixed volume mold),N2 roasting atmosphere,750℃roasting temperature and 10 min holding time,the compressive strength of the prepared foam material exceeds 1.5 MPa,and the volume density is within 0.5 g/cm3.The electromagnetic wave absorption performance of the material is as follows:when the material thickness is 7 mm,the minimum reflectance loss value is-22.14 dB(16.80 GHz),and the effective bandwidth is 1.88 GHz.Its absorption of electromagnetic waves is mainly reflected in the 16~18 GHz frequency band,and the absorption loss mechanism is mainly the magnetic loss effect of ferrite in the gasification slag.It can provide new ideas for the preparation of foam materials and the application of foam materials in the field of electromagnetic wave absorption.

coarse slag from coal water slurry gasificationfoaminglightweightmoldingelectromagnetic wave

谷红伟

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国能销售集团有限公司,北京 100011

水煤浆气化粗渣 发泡 轻质 成型 电磁波

2024

煤炭工程
煤炭工业规划设计研究院

煤炭工程

CSTPCD北大核心
影响因子:0.806
ISSN:1671-0959
年,卷(期):2024.56(12)