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茶叶中铜 镁 钾 锰含量的不确定度评定

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采用湿式消解法-电感耦合等离子体发射光谱法测定茶叶中铜、镁、钾、锰等4种元素的含量,对测定过程中产生的不确定度分量进行了分析和评定,然后计算合成不确定度和扩展不确定度.结果表明,当置信概率为95%,包含因子为2时,茶叶样品中铜含量为4.423 mg/kg,其扩展不确定度为0.046 mg/kg;镁含量为1 769 mg/kg时,其扩展不确定度为0.574 mg/kg;钾含量为45 819 mg/kg时,其扩展不确定度为1.186 mg/kg;锰含量为638 mg/kg,其扩展不确定度为 0.090 mg/kg.
Uncertainty Evaluation of the Content of Cu,Mg,K and Mn in Tea
The contents of Cu,Mg,K and Mn in tea were determined by inductively coupled plasma atomic emission spec-trometry,and the measurement uncertainty was evaluated.The uncertain components was quantified and the combined stan-dard uncertainty and the expanded uncertainty was calculated by the mathematical formula.The results showed that when the confidence level was 95% ,and the coverage factor was 2,the expanded uncertainty was 0.046 mg/kg when the content of Cu was 4.423 mg/kg;the expanded uncertainty was 0.574 mg/kg when the content of Mg was 1 769 mg/kg;the expanded uncer-tainty was 1.186 mg/kg when the content of K was 45 819 mg/kg;the expanded uncertainty was 0.090 mg/kg when the content of Mn was 638 mg/kg.

uncertaintyinductively coupled plasma atomic emission spectrometryteaCuMgKMn

王彬、宋欢、郑晨霞、许娟、罗书美

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信阳师范大学,河南信阳 464000

信阳谭山检测技术有限责任公司,河南信阳 464000

信阳市农业技术服务中心,河南信阳 464000

不确定度 电感耦合等离子体发射光谱法 茶叶

2024

农产品加工
山西省农业机械化科学研究院 山西省农产品加工装备技术管理站 山西省农业产业化协会

农产品加工

影响因子:0.648
ISSN:1671-9646
年,卷(期):2024.(23)