农产品加工2024,Issue(23) :57-60,67.DOI:10.16693/j.cnki.1671-9646(X).2024.23.012

茶叶中铜 镁 钾 锰含量的不确定度评定

Uncertainty Evaluation of the Content of Cu,Mg,K and Mn in Tea

王彬 宋欢 郑晨霞 许娟 罗书美
农产品加工2024,Issue(23) :57-60,67.DOI:10.16693/j.cnki.1671-9646(X).2024.23.012

茶叶中铜 镁 钾 锰含量的不确定度评定

Uncertainty Evaluation of the Content of Cu,Mg,K and Mn in Tea

王彬 1宋欢 2郑晨霞 1许娟 3罗书美2
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作者信息

  • 1. 信阳师范大学,河南信阳 464000
  • 2. 信阳谭山检测技术有限责任公司,河南信阳 464000
  • 3. 信阳市农业技术服务中心,河南信阳 464000
  • 折叠

摘要

采用湿式消解法-电感耦合等离子体发射光谱法测定茶叶中铜、镁、钾、锰等4种元素的含量,对测定过程中产生的不确定度分量进行了分析和评定,然后计算合成不确定度和扩展不确定度.结果表明,当置信概率为95%,包含因子为2时,茶叶样品中铜含量为4.423 mg/kg,其扩展不确定度为0.046 mg/kg;镁含量为1 769 mg/kg时,其扩展不确定度为0.574 mg/kg;钾含量为45 819 mg/kg时,其扩展不确定度为1.186 mg/kg;锰含量为638 mg/kg,其扩展不确定度为 0.090 mg/kg.

Abstract

The contents of Cu,Mg,K and Mn in tea were determined by inductively coupled plasma atomic emission spec-trometry,and the measurement uncertainty was evaluated.The uncertain components was quantified and the combined stan-dard uncertainty and the expanded uncertainty was calculated by the mathematical formula.The results showed that when the confidence level was 95% ,and the coverage factor was 2,the expanded uncertainty was 0.046 mg/kg when the content of Cu was 4.423 mg/kg;the expanded uncertainty was 0.574 mg/kg when the content of Mg was 1 769 mg/kg;the expanded uncer-tainty was 1.186 mg/kg when the content of K was 45 819 mg/kg;the expanded uncertainty was 0.090 mg/kg when the content of Mn was 638 mg/kg.

关键词

不确定度/电感耦合等离子体发射光谱法/茶叶////

Key words

uncertainty/inductively coupled plasma atomic emission spectrometry/tea/Cu/Mg/K/Mn

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出版年

2024
农产品加工
山西省农业机械化科学研究院 山西省农产品加工装备技术管理站 山西省农业产业化协会

农产品加工

影响因子:0.648
ISSN:1671-9646
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