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微波消解-ICP测定硫铁合金中锰含量

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研究应用微波消解处理硫铁样品,通过优化微波消解及ICP光谱仪的工作条件,建立微波消解-ICP法测定硫铁合金中锰含量,其结果的相对标准偏差(RSD,n=6)处于0.42%~0.44%,回收率在98%~108%.实验表明方法快速简便,准确度和精密度满足检测要求.
Determination of Manganese in Ferro-sulfur by ICP-AES with Microwave Digestion
In this paper,microwave digestion of ferro-sulfur samples was studied,and microwave digestion ICP-aes method for the determination of manganese in ferro-sulfur alloy was established by optimizing the working conditions of microwave digestion and ICP spectrometer.The relative standard deviation(RSD,n=6)was 0.42%~0.44%,and the recoveries were 98%~108%.The experimental results show that the method is fast and simple,and the accuracy and precision meet the detection requirements.

microwave digestioninductively coupled plasma emission spectrometrymanganese content

黄合生、邢文青、尚聪亚、傅铁城、吴红兵

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宝武集团中南钢铁广东中南钢铁股份有限公司,广东韶关 512123

微波消解 电感耦合等离子发射光谱法 锰含量

2024

南方金属
广东省金属学会

南方金属

影响因子:0.16
ISSN:1009-9700
年,卷(期):2024.(4)