首页|热处理工艺对尖晶石型Ni0.5Zn0.45Co0.05Fe2O4静磁性能的影响

热处理工艺对尖晶石型Ni0.5Zn0.45Co0.05Fe2O4静磁性能的影响

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利用溶胶凝胶法制备了尖晶石型Ni0.5Zn0.45Co0.05Fe2O4纳米颗粒,设置了3种热处理工艺,发现随着热处理温度的提高,热处理时间的延长,颗粒长大,静磁性能提高.当热处理温度为800℃,保温8 h,材料具有比较好的静磁性能(Ms=30.241Oe,Hc=73.261 emg/g,μ=0.210).另外,将前驱体在磁场条件下热处理,得到颗粒尺寸比同种热处理工艺未加磁场条件下的大,并且静磁性能有了比较大的提高,其比饱和磁化强度甚至比在更高热处理温度,更长热处理时间下制备的NiZnCo铁氧体大.
Effect of Heat Treatment Processing on Static Magnetism Properties of Spinel Ni0.5Zn0.45Co0.05Fe2O4
Spinel Ni0.5Zn0.45Co0.05Fe2O4 nano-particles were prepared using sol-gel method, then heat treated with three different processes. The static magnetism properties were measured by VSM. The results show that increasing heat treated temperature and prolonging heat treated time can do contribution to the improvement of magnetic property. When heat treated in 800℃ for 8h, the material shows high saturation magnetization(Ms=73.261 emu/g) and initial permeability(μi=0.210emu/Oe*g), low coercivity (Hc=30.241Oe). In this work, the effect of magnetic heat treatment on the improvement of static magnetism properties was also studied. The magnetic heated treatment for Ni0.5Zn0.45Co0.05Fe2O4 ferrite could improve its static magnetism properties, the material obtained exhibits high saturation magnetization (Ms=83.839emu/g) even heat treated at relatively low temperature(600℃ for 2h).

NiZnCo-ferritemagnetic heat treatmentstatic magnetism properties

张鑫、顾家琳、康飞宇

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清华大学材料科学与工程系,北京,100084

NiZnCo铁氧体 热处理工艺 静磁性能

2009

纳米科技
西安纳米科技学会 陕西省电子学会纳米技术专业委员会

纳米科技

ISSN:1812-1918
年,卷(期):2009.6(3)
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