农业工程学报2024,Vol.40Issue(6) :72-78.DOI:10.11975/j.issn.1002-6819.202306147

微波真空冷冻干燥时怀山药的微CT孔道分布

Micro-CT pore distribution in Chinese yam under microwave freeze drying

张乐道 李才云 王雅博 任广跃 段续
农业工程学报2024,Vol.40Issue(6) :72-78.DOI:10.11975/j.issn.1002-6819.202306147

微波真空冷冻干燥时怀山药的微CT孔道分布

Micro-CT pore distribution in Chinese yam under microwave freeze drying

张乐道 1李才云 2王雅博 3任广跃 2段续2
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作者信息

  • 1. 内蒙古科技大学生命科学与技术学院,包头 014010;内蒙古自治区生物质能源化利用重点实验室,包头 014010
  • 2. 河南科技大学食品与生物工程学院,洛阳 471023
  • 3. 天津商业大学天津市制冷技术重点实验室,天津 300134
  • 折叠

摘要

局部温度过高的问题限制了微波真空冷冻干燥(microwave freeze drying,MFD)技术在果蔬干燥中的广泛应用.发展传热传质理论是解决MFD局部温度过高问题的根本途径.数值模拟是研究传热传质机理的重要方法,并有望解决MFD中局部温度过高的问题.利用详细的孔径和孔隙分布建立结构模型对数值模拟至关重要.该研究以怀山药为样品,利用微CT(X-ray micro-computed tomography)技术分析不同干燥仓压力(100、200、300 Pa)和微波加载量(0.5、1.0、1.5、2.0W/g)时孔隙和孔隙分布的变化.结果表明,干燥仓内的低压环境更倾向于形成小孔隙,干燥仓内压力的变化对外层的孔隙大小和分布无明显影响,但对内层的孔隙大小和分布有明显影响.微波加载量对内、外层的孔隙大小和分布均有显著影响.研究结果将为解决MFD中局部温度过高问题的数值计算研究提供试验支持.

Abstract

Microwave freeze drying(MFD)can be the rapid removal of water from vegetables and fruits.The quality of dried products can be almost identical to that of conventional freeze drying(FD).MFD can also be expected to potentially replace the conventional FD,particularly for the low cost.However,the excessive local high temperature can result in the local coking during MFD,which has failed to be effectively controlled until now.The excessive local high temperature has restricted the wide range of applications of MFD.In this study,micro-computed tomography(CT)was used to visualize the pore distribution of dried Chinese yam under different microwave loading levels and cavity pressure.A systematic analysis was implemented to determine the pore size and distribution in every partial specimen.The heat and mass transfer mechanism was given for the uneven distribution of temperature during MFD,even for the excessive local temperature.A series of numerical simulations was then carried out to verify the pore size and pore distribution of the structure model.The results indicated that the operation conditions(such as microwave loading level and cavity pressure)shared a significant effect on the pore characteristics of Chinese yam under MFD.There was a distinct distribution in the thickness of the sarcocarp,as the cavity pressure changed.The percentage of 10-50 μm sarcocarp under 200 Pa was higher than that under 100 and 300 Pa.while the percentage of60-160 μm sarcocarp under 200 Pa was lower than that under 100 and 300 Pa.Low microwave loading level tended to form the small pores,whereas,the large pores were observed at high microwave loading level.Low cavity pressure and microwave loading levels tended to form the much smaller pores.The low microwave loading level also induced the smaller pores with a size between 50 and 160 μm.Meanwhile,the high microwave loading level tended to produce much larger pores with sizes between 200 and 550 μm.There was a significant effect of cavity pressure on the pore size and distribution in the inner specimen,whereas,there was no effect in the outer specimen.Therefore,the larger pore was more prone to form in the middle of the sample during MFD.There was a distinct effect of microwave loading level on the pore size and distribution in both the inner and outer layers.The microwave loading level was prone to produce sudden variation in the pore distribution when the pore size was larger than 800 μm.Compared with the cavity pressure,the microwave loading level can be more likely to change the pore size and pore distribution from the inside out,where a lot of large pores were formed in the inner specimen with a size of larger than 800 μm.The finding can also offer experimental support to the numerical simulation for the local high temperature in MFD.

关键词

微波真空冷冻干燥(MFD)/微CT/怀山药/孔道尺寸/孔道分布

Key words

microwave freeze drying(MFD)/Micro-CT/Chinese yam/pore size/pore distribution

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基金项目

国家自然科学基金(52006109)

内蒙古自治区人才引进项目()

内蒙古科技大学基本科研业务费专项(2023QNJS148)

出版年

2024
农业工程学报
中国农业工程学会

农业工程学报

CSTPCD北大核心
影响因子:2.529
ISSN:1002-6819
参考文献量6
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