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UPLC 法测定复配食品添加剂丙酸钙含量

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为避免复配添加剂对滴定结果的干扰,采用高效液相色谱法测定丙酸钙的含量。试验结果表明:丙酸的质量浓度在0.05~1.00 g/L 的范围内与其峰面积呈线性关系,定量限为0.05 g/kg,回收率为97.3%~103.4%,RSD≤2.9%(n=6)。该方法精确度好,灵敏度高,样品预处理简单,是复配食品添加剂中丙酸钙含量测定的理想方法。
Determination of Calcium Propionate in Complex Food Additives by UPLC
UPLC was applied to the determination of calcium propionate in order to avoid the interference of complex food additives on the titration results. The result showed a linear relationship between quality of propionic acid concentration in the range of 0.05 ~ 1.00 g/l and its peak area, in which LOQ was 0.05 g/kg, recovery was 97.3 ~ 103.4% and RSD was less than or equal to 2.9 %(n=6). UPLC was an ideal test method for determination of calcium propionate in complex food additives with its accuracy, high sensitivity, and simple sample pretreatment.

calcium propionateHPLCrecoveryLOQstandard curve

岑琴、李智

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沈阳产品质量监督检验院,沈阳 110022

辽宁大石药业有限公司,辽宁 本溪 117004

丙酸钙 高效液相色谱 回收率 定量限 标准曲线

2014

农业科技与装备
辽宁省农业机械化研究所

农业科技与装备

影响因子:0.319
ISSN:1674-1161
年,卷(期):2014.(9)
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