Determination of Propanil Residues in Rice by Gas Chromatography-Mass Spectrometry
An analytic method was developed to determine the residue of Propanil in rice water,soil,straw,bran and rice samples.The sample was extracted with ethyl acetate and purified by d-SPE,and determined by Gas Chromatography-Mass Spectrometry.The results showed that the average recovery of propanil was 72.3％～108.9％ when spiked at 0.02～2mg/kg,with relative standard deviations of 1.5％～8.2％.Therefore,it was an effective method which met the pesticide residue analysis requirements in sensitivity,accuracy and precision.
NETL
NSTL
万方数据
维普
