首页|基于液相色谱-质谱联用法检测芒果中44种农药及其代谢物残留量的风险分析

基于液相色谱-质谱联用法检测芒果中44种农药及其代谢物残留量的风险分析

扫码查看
以芒果为样品,采用QuEChERS液相色谱-质谱联用法(LC-MS/MS)对芒果中44种农药及其代谢物残留量进行测定,65。0%的全果中检出农药残留。吡唑醚菌酯、苯醚甲环唑在全果中检出率最高,分别为52。5%和35。0%。按照我国制定的最大残留限量标准(MRL),吡唑醚菌酯在全果中存在超标现象,不合格率20%。利用检出的数据进行统计分析,浅析芒果中农药残留量的现状与风险,对加强农药监督管理以及指导种植户合理规范使用农药提出建议,为市场监督管理提供参考。
Risk Analysis of 44 Pesticides and Metabolites Residues in Mango Using Liquid Chromatography-Mass Spectrometry
The residues of 44 pesticides and their metabolites in mango were determined by QuEChERS liquid chromatography-mass spectrometry(LC-MS/MS).Pesticide residues were detected in 65.0%of the whole mango.Among these,pyraclostrobin and difenoconazole exhibited the highest detected rates,found in 52.5%and 35.0%of the whole fruit samples,respectively.The concentration of pyraclostrobin in the whole fruit exceeded the maximum residue limit(MRL)established in China for mangoes,with an unqualified rate of 20%.Through statistical analysis of the detected data,the status quo and associated risks of pesticide residues in mangoes were analyzed.Furthermore,suggestions were put forward to strengthen pesticide supervision and management and to guide farmers to use pesticides in a rational and standardized way,providing references for market supervision and management.

pesticide residuespyraclostrobinmangoliquid chromatography-mass spectrometry

陈丽娥、郭跃平、董晓尉

展开 >

金华市食品药品检验检测研究院,浙江 金华 321015

农药残留 吡唑醚菌酯 芒果 液相色谱-质谱联用法

2024

农药科学与管理
农业部农药检定所

农药科学与管理

CSTPCD
影响因子:0.511
ISSN:1002-5480
年,卷(期):2024.45(2)
  • 9