首页|X射线荧光光谱法测定铝合金中的元素含量

X射线荧光光谱法测定铝合金中的元素含量

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利用X射线荧光光谱特征峰强度与元素含量之间的关系,可确定铝合金中金属元素种类和含量.本试验测量了系列铝合金标准样品(已知金属元素成分含量)X射线荧光光谱(XRF),根据金属元素特征谱线绘制XRF特征峰值与元素含量线性关系曲线.结果表明,使用XRF法检测铝合金中的元素结果准确,灵敏度高,Cu元素质量分数检出限可达3 × 10-6,灵敏度相对低的Ti元素质量分数检出限也可达16×10-6;用XRF法检测了散热铝合金样品中各金属元素含量,其中Cu、Zn的测量结果与激光烧蚀火花诱导击穿光谱法所测结果一致.
Determination of element content in aluminum alloy by X-ray fluorescence spectroscopy
The relationship between the intensity of XRF(X-ray fluorescence spectra)characteristic peak and element content can be used to determine metal element types and contents of aluminum alloys.XRFs of standard samples with known element content were measured and the linear relation ship curves between XRF peaks and element content were plotted based on element characteristic spectrum.The results show that XRF method is accu-rate and sensitive to detect element content.Detection limit of Cu can reach 3 × 10-6,and that of Ti which has relatively low sensitivity can reach 16 × 10-6.The content of various metal elements in the aluminum alloy samples for heat dissipation was detected by XRF method,and the measurement results of Cu and Zn were consistent with those obtained by la-ser ablation spark induced breakdown spectroscopy.

X-ray fluorescence spectroscopy(XRF)aluminum alloymetal elementquantitative analysis

王椿曦、莫境山、熊正烨、张泽锋、王露燕、曾才兴

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广东海洋大学电子与信息工程学院,广东湛江 524088

X射线荧光光谱 铝合金 金属元素 定量分析

湛江市科技计划项目

2022A05022

2024

轻合金加工技术
中国有色金属加工工业协会轻金属分会

轻合金加工技术

影响因子:0.31
ISSN:1007-7235
年,卷(期):2024.52(4)