首页|Al-6.4Zn-2.4Mg-2.05Cu-0.12Zr合金厚板三级时效热处理中的预时效工艺研究

Al-6.4Zn-2.4Mg-2.05Cu-0.12Zr合金厚板三级时效热处理中的预时效工艺研究

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采用DSC、TEM、硬度计等研究了 Al-6.4Zn-2.4Mg-2.05Cu-0.12Zr合金厚板三级时效热处理中的预时效工艺对板材组织性能的影响.结果表明,固溶拉伸自然时效(NA)后的板材晶内析出物以GP区为主,晶界析出相呈链状连续分布,合金硬度约为162 HV.对该自然时效后的板材进行80-140 ℃不同温度预时效,分析预时效温度对晶界和晶内析出相影响.结果表明,随着预时效温度的提高,晶内、晶界析出相尺寸同时长大,在120 ℃24 h预时效,晶内析出相以 η'相为主,硬度最大(189 HV);在140℃24 h预时效,晶内有较多η相析出,硬度衰减.综合考虑组织及性能确定120 ℃24 h为最佳预时效工艺.经实验室和工业化生产验证,最佳预时效工艺处理后的板材性能达到国外同类合金产品水平.
Study on the pre-aging process of Al-6.4Zn-2.4Mg-2.05Cu-0.12Zr alloy thick plate by three-stage aging heat treatment
The effect of pre-aging process on the microstructure and properties of Al-6.4 Zn-2.4Mg-2.05Cu-0.12Zr thick plate during three-stage aging heat treatment was studied with DSC,TEM,hardness tester,etc.The results show that after solution stretching and natural aging(NA),the precipitates are mainly in the GP zone,with continuous chain dis-tribution at grain boundaries and a material hardness of about 162 HV.An analysis was con-ducted on the effects of different pre-aging temperatures ranging from 80 to 140℃on grain boundaries and intragranular precipitates in the naturally aged plate.The results indicate that with the increase of pre-aging temperature,the size of precipitates inside grains and at grain boundaries grows simultaneously.Pre-aged at 120 ℃ for 24 hours,the intragranular precipi-tated phase is mainly composed of the η'phase,and the hardness reaches highest(189 HV).Pre-aged at 140℃for 24 hours,more η phases precipitate and leads to a decrease in hardness.The optimal pre-aging process is determined to be 120 ℃ for 24 hours based on comprehensive structure and performance of the plates.It has been verified in the laboratory and industrial production,and the processed plates have reached the same performance level of similar alloy products abroad.

three-stage agingpre-ageingGP zoneVickers hardness

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中国铝业集团高端制造股份有限公司,重庆 400000

三级时效 预时效 GP区 维氏硬度

2024

轻合金加工技术
中国有色金属加工工业协会轻金属分会

轻合金加工技术

影响因子:0.31
ISSN:1007-7235
年,卷(期):2024.52(8)