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气相色谱法测定气体中微量硫化物含量

DISCUSSION ON THE DETERMINATION OF TRACE SULFIDE IN GAS BY GAS CHROMATOGRAPHY

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采用气相色谱法测定气体中的微量硫化物含量,对比分析了普通玻璃针筒充氮进样和交叉式标准气体预混合进样两种稀释方法,并在样品分析的注意事项等方面提出了可靠性的建议.结果表明:交叉式标准气体预混合进样方法具有更高的可靠性和精度,可以满足实验要求,该方法具有灵敏度高、重复性好、操作简单等优点,可满足气体中微量硫化物含量的测定需求.
Trace sulfide content in gases was determined by Gas chromatography.Two dilu-tion methods of ordinary glass syringe nitrogen injection and cross type standard gas premixed in-jection used for sample injection were compared and analyzed,and reliable suggestions about precautions in course of sample analysis were proposed.The results showed that the cross type standard gas premixed injection method possessed higher reliablity and precision,which could meet experiment condition.On the other hand,the method had the following advantages,such as high sensitivity,good repeatability,simple operation,etc.,which was practical for conduc-ting inspection and analysis work.

trace sulfidechromatographydetermination

赵文波、巩亚威、周发海

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河南龙宇煤化工有限公司,河南永城 476600

微量硫化物 色谱法 测定

2024

齐鲁石油化工
齐鲁石油化工公司研究院

齐鲁石油化工

影响因子:0.259
ISSN:1009-9859
年,卷(期):2024.52(4)