热带农业科学2024,Vol.44Issue(8) :65-74.DOI:10.12008/j.issn.1009-2196.2024.08.011

辅助降血糖茄皮含片制备

The Optimization Process of Formula for Solanum melongena Peels

郭子斌 魏静 范蓓 王凤忠 蔡如玉 孙晶
热带农业科学2024,Vol.44Issue(8) :65-74.DOI:10.12008/j.issn.1009-2196.2024.08.011

辅助降血糖茄皮含片制备

The Optimization Process of Formula for Solanum melongena Peels

郭子斌 1魏静 2范蓓 2王凤忠 2蔡如玉 2孙晶1
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作者信息

  • 1. 山西农业大学/山西省农业科学院食品科学与工程学院 山西 晋中 030600;中国农业科学院农产品加工研究所/农业农村部农产品加工质量安全风险评估实验室/农业农村部农产品质量安全收贮运管控重点实验室 北京 100193
  • 2. 中国农业科学院农产品加工研究所/农业农村部农产品加工质量安全风险评估实验室/农业农村部农产品质量安全收贮运管控重点实验室 北京 100193
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摘要

以茄皮提取物(Solanum melongena peels extract,SMPE)酚类物质为基础,利用单因素试验结合Box-Behnken响应面设计实验得到最优茄皮含片配方工艺.实验采用超高效液相色谱串联质谱(ultra performance liquid chromatog-raphy tandem mass spectrometry,UPLC-MS/MS)测定紫黑色和紫红色茄皮SMPE中酚类物质含量,筛选出最优原材料,然后利用 Box-Behnken 响应面设计试验考察 SMPE、甘露醇、木糖醇和柠檬酸添加量对综合感官评分的影响,确定最优复配工艺.结果表明,紫黑色茄皮多酚总量为 52.7 mg/g,高于紫红色茄皮 37.4 mg/g,故优选紫黑色茄皮为提取原材料.茄皮含片优化复配工艺为SMPE 30%、木糖醇 16%、甘露醇 12%、柠檬酸 2.5%,综合感官评分为 92.7,与模型理论预测值 93.0 基本吻合(RSD=0.200%),经优化复配的茄皮含片风味口感适宜,保证了茄皮含片在辅助降血糖功效方面的应用.

Abstract

Using the phenolic compounds of Solanum melongena peel extract(SMPE)as a basis,the optimal formula and process for producing eggplant skin tablets were determined through single-factor experiments combined with Box-Behnken response surface design experiments.Ultra Performance Liquid Chromatography-Tandem Mass Spectrometry(UPLC-MS/MS)was used to determine the content of phenolic compounds in purple-black and purple-red SMPE,and the optimal raw materials were screened.Then,Box-Behnken response surface design experiments were subsequently conducted to investigate the ef-fects of SMPE,mannitol,xylitol,and citric acid on the comprehensive sensory score,and the optimal compound technology was determined.The results revealed that the total polyphenol content of purple-black eggplant peel was 52.7 mg/g,which was higher than that of purple-red eggplant peel(37.4 mg/g);thus,so purple-black eggplant peel was selected as the extraction raw material.The optimized compound technology for eggplant peel tablets was SMPE 30%,xylitol 16%,mannitol 12%,and citric acid 2.5%,and the comprehensive sensory score was 92.7,which was consistent with the theoretical prediction value of the model(RSD=0.200% ).The optimized eggplant peel tablets had a suitable flavor and taste,ensuring the application of eggplant peel tablets in assisting blood glucose reduction.

关键词

茄皮提取物/多酚/含片/响应面法/超高效液相色谱-串联质谱

Key words

Solanum melongena peel extract/polyphenols/lozenges/response surface method/ultra-performance liquid chromatography-tandem mass spectrometry

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基金项目

国家重点研发计划(2022YFC2010104)

中国农业科学院农产品加工研究所创新工程院所重点任务(CAAS-ASTIP-G2022-IFST-04)

出版年

2024
热带农业科学
中国热带农业科学院

热带农业科学

CSTPCD
影响因子:0.534
ISSN:1009-2196
参考文献量31
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