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市售红茶中农药残留检测与健康风险评价

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调查从福建市场中采集的 160 份红茶样品中 65 种农药残留的浓度,并评估在饮茶过程中的健康风险.采用气相色谱—质谱法和液相色谱—质谱法进行农药残留检测与分析,依据《食品安全国家标准 食品中农药最大残留限量》(GB 2763-2021)对结果进行判定.结果表明,65 种已知农药残留中检测到 28 种,检出农药残留样品 115 份,检出率71.87%,检出农药残留值均低于国家允许最大残留限量值,合格率 100%.检出率呋虫胺(60.63%)>唑虫酰胺(58.13%)>吡虫啉(50%)>丁醚脲(48.75%)>啶虫脒(39.38%)>噻虫嗪(25.63%)>联苯菊酯(20%).农药残留的急性和慢性风险熵研究表明,HQ值均远小于 100%,由茶叶中引入的农药残留风险不会对消费者健康造成威胁,但唑虫酰胺aHI达急性参考计量的 31.5%,急性膳食风险应加以关注.
Detection and Health Risk Assessment of Pesticide Residues in Commercially Available Black Tea
The primary objective of this study was to scrutinize the presence and levels of 65 pesticide residues in 160 black tea samples sourced from the Fujian market and conduct an assessment of the potential health risks associated with the con-sumption of these teas.The analysis included employing both gas chromatography-mass spectrometry and liquid chromatog-raphy-mass spectrometry to detect and quantify pesticide residues,with evaluations based on the"National Food Safety Stan-dard-Maximum Residue Limits of Pesticides in Food"(GB 2763-2021).The results revealed that out of the 65 known pesti-cide residues,28 were detected in the tea samples.Among the 160 samples examined,115 were found to contain pesticide residues,resulting in a detection rate of 71.87%,all of which were lower than the national maximum residue limit,and a 100%pass rate was reached.Notably,the pesticides most frequently detected included dinotefuran(60.63%),pyramiprid(58.13%),imidacloprid(50%),difenthiuron(48.75%),acetamiprid(39.38%),thiamethoxam(25.63%),and bifenthrin(20%).Further-more,according to an acute and chronic risk entropy study of pesticide residues,the computed hazard quotient(HQ)values were substantially below the critical threshold of 100,indicating that pesticide residues in tea does not represent a significant health threat for consumers.However,notably,the acute hazard index(aHI)for pyrimidines reached 31.5%of the acute ref-erence level,signifying the acute dietary risk should be noted.

black teapesticide residuegas chromatography-mass spectrometryliquid chromatography-mass spectrometryrisk assessment

胡汉亮、吴清莲、蔡清毅、李杨、李金贵、李奠础

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漳州科技职业学院 福建 漳州 363202

漳州市休闲食品产业技术研究院 福建 漳州 363202

闽台食品加工及安全福建省高校应用技术工程中心 福建 漳州 363202

红茶 农药残留 气相色谱—质谱法 液相色谱—质谱法 风险评估

2024

热带农业科学
中国热带农业科学院

热带农业科学

CSTPCD
影响因子:0.534
ISSN:1009-2196
年,卷(期):2024.44(10)