首页|8英寸半导电型GaAs单晶衬底的制备与性能表征

8英寸半导电型GaAs单晶衬底的制备与性能表征

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本文使用垂直梯度凝固(VGF)法制备了直径超过200 mm的Si掺杂GaAs单晶.通过多线切割、磨边、研磨、化学机械抛光和湿法化学清洗等加工工序制备出8英寸半导电型GaAs单晶衬底.使用X射线衍射、位错密度检测、霍尔测试、非接触式表面电阻率测试、光致发光测试和晶圆表面缺陷检测等对8英寸GaAs衬底的晶体质量、位错、电学性能和表面质量等特性进行了测试分析.结果表明:衬底(400)衍射峰半峰全宽低于0.009°;平均位错密度低于30 cm-2,其中,晶体头部平均位错密度为1.7 cmI-2,且有98.87%的面积位错密度为0;衬底面内电阻率标准差小于6%,面内光致发光强度标准差小于4%,≥0.2 μm的表面光点缺陷(LPD)个数小于10.上述结果表明,所制备的8英寸GaAs衬底质量优异,满足外延器件对高质量衬底的要求.
Fabrication and Characterization of 8 Inch Semiconducting GaAs Single Crystal Substrate
Si doped GaAs single crystal with diameter over 200 mm was prepared by vertical gradient freeze(VGF)method.The 8 inch GaAs single crystal substrate was obtained through multi-line cutting,edging,grinding,chemical mechanical polishing and wet cleaning.The crystal quality,dislocation density,electrical properties and surface quality of 8 inch GaAs substrate were characterized by X-ray diffraction,dislocation density inspection,Hall measurement,non-contact surface resistivity measurement,photoluminescence and wafer surface defect inspection.The results show that the full width of half maximum(FWHM)of substrate(400)diffraction peak is smaller than 0.009°,the average dislocation density is lower than 30 cm-2,the lowest dislocation density is 1.7 cm-2and 98.87%area are zero dislocation.Moreover,the standard deviation of surface resistivity and photoluminescence intensity are smaller than 6%and 4%,respectively.The number of the spot with light point defect(LPD)≥0.2 μm is less than 10.The results show that the 8 inch semiconducting GaAs single crystal substrate with excellent performance is developed and can be used as the high quality substrate for epitaxial growth and devices fabrication.

GaAsvertical gradient freeze8 inchsingle crystal substratedislocation density

任殿胜、王志珍、张舒惠、王元立

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北京通美晶体技术股份有限公司,北京 101113

GaAs 垂直梯度凝固 8英寸 单晶衬底 位错密度

2024

人工晶体学报
中材人工晶体研究院

人工晶体学报

CSTPCD北大核心
影响因子:0.554
ISSN:1000-985X
年,卷(期):2024.53(3)
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