首页|Yb∶Lu2O3透明陶瓷的制备及激光性能研究

Yb∶Lu2O3透明陶瓷的制备及激光性能研究

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稀土离子掺杂的倍半氧化物陶瓷材料具有高热导率、低声子能量、高激光损伤阈值等优势,在固体激光领域具有巨大的应用潜力。本文采用化学共沉淀法合成了高纯度、低团聚Yb∶Lu2O3陶瓷粉体,在氧气气氛下预烧后,结合热等静压(HIP)烧结制备了具有高致密度、高透过率的5%(原子数分数)Yb∶Lu2O3透明陶瓷。陶瓷的平均晶粒尺寸小于1 μm,在1 100 nm波长处的透过率超过81%。在974 nm波长处吸收截面为~0。97 × 10-20 cm2,在1。08 μm波长处的发射截面为~0。39×10-20 cm2。采用976 nm半导体激光器泵浦Yb∶Lu2O3陶瓷,室温条件下实现了 11。67 W的连续激光输出,对应的斜效率为55。3%,激光中心波长为1 080。1 nm。
Fabrication and Laser Performance of Yb∶Lu2O3 Transparent Ceramics
Rare-earth ions doped sesquioxide ceramics exhibit notable advantages,including high thermal conductivity,low phonon energy,and high laser damage threshold,thereby demonstrating significant potential for solid-state laser applications.Powders with high purity and low agglomeration were synthesized by chemical co-precipitation method,then 5%(atomic fraction)Yb∶Lu2O3 transparent ceramics with high density and high transparency were obtained through oxygen pre-sintering and hot isostatic pressing(HIP)sintering.The samples have an average grain size of less than 1 μm,and exhibit an in-line transmittance of above 81%at 1 100 nm.The absorption cross-section at 974 nm is~0.97×10-20 cm2,and the emission cross-section at 1.08 µm is~0.39×10-20 cm2.Using a 976 nm laser diode as the pump source,a continuous-wave(CW)laser output at 1 080.1 nm is achieved from the fabricated Yb∶Lu2O3 ceramics at room temperature,with a output power of 11.67 W and slope efficiency of 55.3%.

Yb∶Lu2O3sesquioxidetransparent ceramicsspectral analysislaser performance

李晴、姜珍兴、王莹、马杰、王俊、刘鹏、章健、范金太、于浩海、张怀金、唐定远

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山东大学,晶体材料国家重点实验室,济南 250100

江苏师范大学,江苏省先进激光材料与器件重点实验室,徐州 221116

中国科学院上海硅酸盐研究所,上海 201899

中国科学院上海光学精密机械研究所,上海 201800

深圳技术大学未来技术学院,深圳 518118

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Yb∶Lu2O3 倍半氧化物 透明陶瓷 光谱分析 激光性能

2024

人工晶体学报
中材人工晶体研究院

人工晶体学报

CSTPCD北大核心
影响因子:0.554
ISSN:1000-985X
年,卷(期):2024.53(11)