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ICP-AES法测定炼钢用增碳剂中二氧化钛含量

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通过碳酸钠、四硼酸钠等碱性混合助熔剂熔解增碳剂试样,用盐酸、热水熔解熔球,过滤得到稳定的待测溶液.使用电感耦合等离子体发射光谱法,测定待测元素的光谱强度,从而得到其含量.实验表明:本法较灰分成分分析,无须检测灰分,分析快速,方法的精密度和正确度满足要求.
Determination of Titanium Dioxide in Carburizer for Steelmaking by ICP-AES
To test the content of titanium dioxide in carburizer for steelmaking,the sample was prepared by process of alkali fusung with mixed fluxing agent,hot water and hydrochloric acid acidification.The fluxing agent composed of sodium carbonate and sodium tetrahorate.A stable solution to he tested was obtained by filtration.The spectral intensity of the element to he measured was determined by inductively coupled plasma emission spectrometry.The experiment shows that this method does not need to detect the ash content,and the analysis is faster,compared to the ash component analysis.The precision and accuracy of the method can meet the requirements.

carburanttitanium dioxideinductively coupled plasma emission spectrometry

张延新、高立杰、吕艳艳、刘爽

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青岛特殊钢铁有限公司质量检测所,山东 青岛 266000

增碳剂 二氧化钛 电感耦合等离子体发射光谱法

2024

山东冶金
山东金属学会

山东冶金

影响因子:0.176
ISSN:1004-4620
年,卷(期):2024.46(5)