山东冶金2024,Vol.46Issue(5) :44-46.

质量平衡法测定正十六烷纯度

Determination of n-cetane Purity by Mass Balance Method

王庆栋
山东冶金2024,Vol.46Issue(5) :44-46.

质量平衡法测定正十六烷纯度

Determination of n-cetane Purity by Mass Balance Method

王庆栋1
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作者信息

  • 1. 山东省冶金科学研究院有限公司,山东 济南 250102
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摘要

质量平衡法是基于被测物质质量分数总和为100%的前提下(全部杂质未知),通过气相色谱面积归一法计算正十六烷的有机纯度,卡尔·费休库伦法测定水分含量,色谱法测定挥发组分的含量,ICP-MS测定不挥发组分的含量.扣除测得杂质后,即得正十六烷的纯度.该方法为纯度定值的基准方法、广泛应用于正十六烷等有机物的纯度定值.

Abstract

Mass balance method is based on the premise that the total mass fraction of the tested substance is 100%,the organic purity of n-cetane is calculated by gas chromatography area normalization method,the water content is determined by Carl Fischcullen method,the volatile component content is determined by chromatography,and the non-volatile component content is determined by ICP-MS.After deducting the measured impurities,the purity of n-cetane is obtained.This method is the standard method of purity determination,and is widely used in the purity determination of n-hexadecane and other organic compounds.

关键词

质量平衡法/正十六烷/纯度

Key words

mass balance method/n-cetane/purity

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出版年

2024
山东冶金
山东金属学会

山东冶金

影响因子:0.176
ISSN:1004-4620
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