山东冶金2024,Vol.46Issue(6) :37-38,41.

气相色谱法检测丙酮中除草醚分析方法优化及确认

Method for Determination of Herbicides in Acetone Was Established

刘君丽
山东冶金2024,Vol.46Issue(6) :37-38,41.

气相色谱法检测丙酮中除草醚分析方法优化及确认

Method for Determination of Herbicides in Acetone Was Established

刘君丽1
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作者信息

  • 1. 山东省冶金科学研究院有限公司,山东济南 250102
  • 折叠

摘要

本文研究了丙酮中除草醚溶液标准物质在研制过程中,采用气相色谱法检测时,通过改变进样口温度、分流比和程序升温条件等不同参数对分析方法进行了优化.并进行了方法确认,经确认,该分析方法仪器测定时随机误差较小,相对标准偏差小于2%,精密度及线性良好,可以用作丙酮中除草醚溶液标准物质的均匀性检验、稳定性检验的分析方法.

Abstract

In this paper,the determination of reference materials in acetone by Gas chromatography was studied.The method was validated by changing the inlet temperature,the split ratio and the temperature-programmed conditions.It is confirmed that the method has a good precision and linearity with a small random error and a relative standard deviation of less than 2%,it can be used as the analysis method of homogeneity test and stability test for the reference material of herbicide solution in acetone.

关键词

除草醚/溶液标准物质/气相色谱

Key words

nitrofen/solution reference material/gas chromatography

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出版年

2024
山东冶金
山东金属学会

山东冶金

影响因子:0.176
ISSN:1004-4620
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