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用空白焙烧 酸浸工艺从石煤钒矿中提取钒

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研究了采用空白焙烧—酸浸工艺从某石煤钒矿中提取钒,考察了磨矿细度、焙烧时间、焙烧温度、硫酸用量、助浸剂CaF2用量、浸出温度、浸出时间和液固体积质量比对钒浸出率的影响.结果表明:适宜的空白焙烧条件为磨矿细度-74 μm占70%,焙烧温度775 ℃和焙烧时间5 h;适宜的酸浸条件为硫酸用量10%、助浸剂CaF2用量3%,液固体积质量比1.5∶1,浸出温度25 ℃和浸出时间1.5 h;适宜条件下,钒浸出率可达81.5%.
Leaching of Vanadium from Stone Coal Vanadium Ore by Blank Roasting-Acid Leaching Process
Leaching of vanadium from stone coal vanadium ore by blank roasting-acid leaching process was studied.The effects of grinding fineness,roasting time,roasting temperature,sulfuric acid addition dosage,leaching aid CaF2 addition dosage,leaching temperature,leaching time and liquid volume to solid mass ratio on vanadium leaching rate were investigated.The results show that the optimum blank roasting conditions are grinding fineness 70%of-74 μm,roasting temperature of 775 ℃ and roasting time of 5 h.The optimum acid leaching conditions are sulfuric acid addition dosage of 10%,leaching aid CaF2 addition dosage of 3%,liquid volume to solid mass ratio of 1.5:1,leaching temperature of 25 ℃ and leaching time of 1.5 h.Under suitable conditions vanadium leaching rate can reach 81.5%.

stone coal vanadium oreblank roastingacid leachingsulfuric acidvanadium

王祥、吴天娇

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西安西北有色地质研究院有限公司,陕西 西安 710054

陕西省矿产资源综合利用工程技术研究中心,陕西西安 710054

石煤钒矿 空白焙烧 酸浸 硫酸

2024

湿法冶金
核工业北京化工冶金研究院

湿法冶金

北大核心
影响因子:0.631
ISSN:1009-2617
年,卷(期):2024.43(3)
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