Determination of Arsenic Content in Phosphorus Pentoxide by Atomic Fluorescence Spectroscopy Method
The determination of arsenic content in phosphorus pentoxide by atomic fluorescence spectroscopy method was studied,and the acid medium,acidity,reducing agent concentration,pre reducing agent,and masking agent were determined.The results indicate that the method has good linearity in the range of 1.0～50.0 μg/L,the correlation coefficient is r＞0.999,the detection limit is 0.06 μg/L,quantification limit is 0.21 μg/L.The relative standard deviation(RSD)of the 8 sample analysis results is 1.94％,and the spiked recovery rate are 92.87％～101.30％.The test results show no significant difference from the DDTC silver salt method,and this method is a reliable method for detecting arsenic content in phosphorus pentoxide,because it is more convenient and less reagent used.
atomic fluorescence spectroscopy methodDDTC silver salt methodphosphorus pentoxidearsenicdeterminationanalyzation
万方数据
维普
