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溶胶-凝胶法制备钛酸钡纳米粉体

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以钛酸四丁酯和乙酸钡为原料,乙醇和乙酸为溶剂,采用溶胶-凝胶法制备了钛酸钡纳米粉体,并通过XRD、SEM、TG-DTA分析,确定最优工艺条件为:凝胶化温度 70℃,混合溶液pH值为 3.0~4.0,热处理温度 800℃,可获得粒径在50 nm左右的单一钙钛矿相钛酸钡粉体.
Preparation of Barium Titanate Nanoparticles by Sol-gel Method
Using tetrabutyl titanate and barium acetate as raw materials,ethanol and acetic acid as solvents,barium titanate nano powders were prepared by sol-gel method.Through XRD,SEM and TG-DTA analysis,the optimal process conditions were determined as follows:gel temperature 70℃,pH value of mixed solution 3.0~4.0,and heat treatment temperature 800℃.A single perovskite phase barium titanate powder with a particle size of about 50 nm could be obtained.

sol-gel methodbarium titanatepowder

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中国原子能科学研究院, 北京 102413

溶胶-凝胶法 钛酸钡 粉体

2024

山西化工
山西省煤化工发展促进中心 山西省化工学会

山西化工

影响因子:0.293
ISSN:1004-7050
年,卷(期):2024.44(1)
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