基于F-C反应合成多种二乙酰基单体
Synthesis of Multiple Diacetyl Monomers Based on F-C Reaction
曾梦婷 1黎明1
作者信息
- 1. 湖北大学化学化工学院, 湖北 武汉 430062
- 折叠
摘要
在酰基化催化剂存在的条件下,二苯基化合物和乙酰氯发生F-C酰基化反应,生成二乙酰基单体.在文献的基础上,变换二苯基化合物的结构,探究反应可行性和产率.本方法反应条件温和,步骤简单,产率极高,反应产物经核磁和红外等表征方式确定结构.
Abstract
In the presence of acylation catalysts,diphenyl compounds undergo F-C acylation reaction with acetyl chloride,generating diacetyl monomers.On the basis of literature,this paper transforms the structure of diphenyl compounds to explore the feasibility and yield of the reaction.This method has mild reaction conditions,simple steps,and extremely high yields.The structure of the reaction product is determined by characterization methods such as nuclear magnetic resonance and infrared spectroscopy.
关键词
F-C反应/合成/二乙酰基单体/二苯基化合物/纯化Key words
F-C reaction/synthesis/diacetyl monomer/diphenyl compounds/purification引用本文复制引用
出版年
2024
NETL
NSTL
维普
万方数据