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石楠藤无机元素指纹图谱的建立及相关性分析

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目的:分析江西不同产地石楠藤的 20 种无机元素含量,绘制石楠藤无机元素指纹图谱,为石楠藤质量评价提供基础数据.方法:以采自江西省新余市、宜春市上高县、新余市分宜县、宜春市高安市、宜春市三阳县的石楠藤样品为实验材料,采用微波消解-ICP-OES/MS法测定分析Li、Be、Ti、V、Cr、Co、Ni、Zn、Ga、Sr、Sn、Sb、Ba、Tl、Bi、Mg、K、Fe、Mn、Ca元素含量,绘制无机元素指纹图谱,并进行相关性分析.结果:石楠藤中含有大量的无机元素,其中Ca含量最高,平均值达 8872.893 mg/kg;其次是Mg,平均值 7982.388 mg/kg;含量最低的是Be,为 0.015~0.031 mg/kg.不同产地无机元素含量有较大差别,但Ca、Ti、Be、V、Li、Co、Ga的含量较为平均.根据无机元素的含量,绘制石楠藤无机元素指纹图谱,并进行相关性分析.结果显示,有 4 对元素显示显著正相关,10 对元素显示显著负相关,1 对元素显示极显著负相关.结论:石楠藤中无机元素含量丰富,无机元素指纹图谱可用于鉴别石楠藤,结果可为石楠藤的质量控制和安全使用提供参考依据.
Establishment of Inorganic Element Fingerprint of Piper Puberulum and Correlation Analysis
Objective:To analyze the content of 20 inorganic elements in Piper puberulum from different regions in Jiangxi,and draw a fingerprint of inorganic elements in Piper puberulum,in order to provide basic data for quality evaluation of Piper puberulum.Methods:The contents of Li,Be,Ti,V,Cr,Co,Ni,Zn,Ga,Sr,Sn,Sb,Ba,Tl,Bi,Mg,K,Fe,Mn,Ca were determined by microwave digestion combined with inductively coupled plasma mass spectrometry,and the inorganic element fingerprints were drawn,and correlation analysis was conducted.Result:The Piper puberulum contains a large amount of inorganic elements,with the highest content of Ca,with an average value of 8 872.893 mg/kg;Next is Mg,with an average value of 7982.388 mg/kg.The lowest content is Be,ranging from 0.015 to 0.031 mg/kg.There are significant differences in the content of inorganic elements among different regions,but the content of Ca,Ti,Be,V,Li,Co,and Ga is relatively average.Based on the content of inorganic elements,draw a fingerprint of inorganic elements in Piper puberulum and conduct correlation analysis.The results showed that 4 pairs of elements showed significant positive correlation,10 pairs showed significant negative correlation,and 1 pair showed extremely significant negative correlation.Conclusion:The content of inorganic elements in Piper puberulum is abundant,and the fingerprint of inorganic elements can be used to identify Piper puberulum.The results can provide a reference basis for quality control and safe use of Piper puberulum.

Piper puberuluminorganic elementfingerprint spectrum

包鹏杰

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宁波卢米蓝新材料有限公司, 浙江 宁波 315048

石楠藤 无机元素 指纹图谱

2024

山西化工
山西省煤化工发展促进中心 山西省化工学会

山西化工

影响因子:0.293
ISSN:1004-7050
年,卷(期):2024.44(1)
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