山西化工2024,Vol.44Issue(2) :75-77.DOI:10.16525/j.cnki.cn14-1109/tq.2024.02.026

吹扫捕集/气相色谱-质谱法测定生活饮用水中苯甲醚、二溴乙烯、五氯丙烷

Determination of Benzyl Ether,Dibromoethylene,and Pentachloropropane in Drinking Water by Purge Trap/Gas Chromatography-Mass Spectrometry

赵静
山西化工2024,Vol.44Issue(2) :75-77.DOI:10.16525/j.cnki.cn14-1109/tq.2024.02.026

吹扫捕集/气相色谱-质谱法测定生活饮用水中苯甲醚、二溴乙烯、五氯丙烷

Determination of Benzyl Ether,Dibromoethylene,and Pentachloropropane in Drinking Water by Purge Trap/Gas Chromatography-Mass Spectrometry

赵静1
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作者信息

  • 1. 山西省地质集团检测技术有限公司, 山西 太原 030001
  • 折叠

摘要

建立了吹扫捕集/气相色谱-质谱法测定生活饮用水中苯甲醚、二溴乙烯、五氯丙烷的方法,检测方式为全扫描(SCAN),扫描离子范围是 35~270 u.经过对吹扫时间、吹扫温度、升温程序等一系列参数的优化,使目标物的峰形良好、精密度和准确度良好,并且得到较低的检出限.本方法适用于生活饮用水中苯甲醚、二溴乙烯、五氯丙烷3 种挥发性有机物的测定.

Abstract

A purge capture/gas chromatography-mass spectrometry method was established for the determination of anisole,dibromoe-thylene,and pentachloropropane in drinking water.The detection method was full scan(SCAN),with a scanning ion range of 35~270u.After optimizing a series of parameters such as blowing time,blowing temperature,and heating program,the peak shape of the target substance was good,with good precision and accuracy,and a lower detection limit was obtained.This method is applicable to the determination of three volatile organic compounds in drinking water,namely anisole,dibromoethylene,and pentachloropropane.

关键词

吹扫捕集/挥发性有机物/气相色谱-质谱

Key words

purge and capture/volatile organic compounds/gas chromatography-mass spectrometry

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出版年

2024
山西化工
山西省煤化工发展促进中心 山西省化工学会

山西化工

影响因子:0.293
ISSN:1004-7050
参考文献量5
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