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纳氏试剂分光光度法测定氨氮前处理探讨及改进

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依据《水质 氨氮的测定 纳氏试剂分光光度法》(HJ 535-2009)方法中常用的水样前处理方法,通过比较直接比色、絮凝沉淀取上清液、絮凝沉淀过滤、絮凝沉淀离心 4 种方法测定的结果,确定了最为合适的前处理方法.同时,本研究也探索、调整了取样体积和试剂使用量的可行性,达到了简化操作的目的,从而确保测定结果准确性,给同行带来数据参考.
Discussion and Improvement on Pretreatment Methods for Determination of Ammonia Nitrogen in Water by Nessler's Reagent Spectrophotometry
In this study,the most suitable pretreatment method for ammonia nitrogen was determined by comparing the results of four methods direct colorimetry,flocculation and precipitation of supernatant,flocculation and precipitation filtration,and flocculation and precipitation centrifugation,based on the methods of Water quality-Determination of Ammonia nitrogen-Nessler's Reagent Spectrophotometry(HJ 535-2009).Meanwhile,this study also solved the problem of low supernatant volume in actual operation,explored and adjusted the feasibility of sampling volume and reagent usage to achieve the purpose of simplifying the operation,thus ensuring the accuracy of the determination results and bringing data reference to colleagues.

Nessler's reagent spectrophotometryammonia nitrogenpretreatmentsample volume

刘君、于月

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江苏省镇江环境监测中心,江苏 镇江 212000

纳氏试剂分光光度法 氨氮 前处理 取样体积

2024

山西化工
山西省煤化工发展促进中心 山西省化工学会

山西化工

影响因子:0.293
ISSN:1004-7050
年,卷(期):2024.44(3)
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