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水性涂料中甲醛测试方法改进

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建立简便快速且准确的测定水性涂料中甲醛的方法.采用改进的平行合成仪(6 位)一次可以测试 3组 6个样品.用蒸馏水吸收蒸馏出的甲醛,使用乙酰丙酮分光光度计法测定.采用此方法可以把样品的蒸馏时间从60 min缩短至20 min,一次可以平行蒸馏3组6个样品,操作简便,平行性好.方法相对标准偏差为0~5%,回收率为95%~105%.本方法操作简便、快速、准确、高效,具有良好的分析应用前景,可满足实验室大批次涂料的甲醛检测工作要求.
Improvement of Formaldehyde Testing Method in Waterborne Coatings
Establish a simple,fast,and accurate method for the determination of formaldehyde in water-based coatings.This article uses an improved parallel synthesizer that can test three sets of six samples at once.Absorb the distilled formaldehyde with distilled water and determine it using acetylacetone spectrophotometer method.By using this method,the distillation time of the sample can be shortened from 60 minutes to 20 minutes,and three groups of six samples can be distilled in parallel at once.The operation is simple and the parallelism is high.The relative standard deviation of the method is 0~5%,and the recovery rate is 95%~105%.This method is easy to operate,fast,accurate,and efficient,with good analytical application prospects,and can meet the requirements of formaldehyde detection in large batches of coatings in the laboratory.

formaldehydewaterborne coatingsdetermination

韩丹

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立邦涂料(中国)有限公司,上海 201201

甲醛 水性涂料 检测

2024

山西化工
山西省煤化工发展促进中心 山西省化工学会

山西化工

影响因子:0.293
ISSN:1004-7050
年,卷(期):2024.44(6)