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有机硅改性酚醛树脂复合材料制备及性能研究

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本文开展了有机硅改性酚醛树脂复合材料制备及性能研究.首先进行有机硅改性酚醛树脂复合材料的制备:将 4g甲基苯基二甲氧基硅烷溶于 25 mL四甲基氢氧化铵中,然后将得到的料液添至去离子水中进行搅拌,得到黄色固体,并将其置于 60℃烘箱中,设置时间 24 h,得出有机硅改性酚醛树脂复合材料.再者,对有机硅改性酚醛树脂复合材料的热性能及复合材料层间剪切强度进行测试.研究结果表明:当固化环氧树脂和固化剂质量比为95∶5 时,有机硅改性酚醛树脂复合材料性能最优,此时其层间剪切强度高达 87.5 MPa,热失重质量为 0.22 g,耐热性能更好.
Preparation and Properties of Organosilicon Modified Phenolic Resin Composite Materials
This article investigates the preparation and properties of organic silicon modified phenolic resin composite materials.Firstly,prepare the organic silicon modified phenolic resin composite material.Dissolve 4 g of methylphenyldimethoxysilane in 25 mL of tetramethylammonium hydroxide,then add the resulting solution to deionized water and stir to obtain a yellow solid.Place it in a 60℃oven for 24 hours to obtain the organic silicon modified phenolic resin composite material.Furthermore,the thermal properties and interlayer shear strength of organosilicon modified phenolic resin composite materials were tested.The research results show that when the mass ratio of cured epoxy resin to curing agent is 95:5,the performance of the organic silicon modified phenolic resin composite material is optimal.At this time,its interlayer shear strength is as high as 87.5 MPa,the thermal weight loss mass is 0.22 g,and the heat resistance is better.

organosiliconmodificationphenolic resincompound materialpreparationperformance

孙晓东

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酒泉职业技术学院,甘肃 酒泉 735000

有机硅 改性 酚醛树脂 复合材料 制备 性能

2024

山西化工
山西省煤化工发展促进中心 山西省化工学会

山西化工

影响因子:0.293
ISSN:1004-7050
年,卷(期):2024.44(8)