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探讨影响异狄氏剂在气相色谱中降解因素

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异狄氏剂是一种常见的有机氯农药之一,本文利用气相色谱法(GC-ECD)考察了影响异狄氏剂降解的因素,并确定在脉冲不分流进样模式下,进样口温度为 280℃时,首选超高惰带玻璃纤维衬管 5190-2293 和不黏连的流失与温度优化BTO隔垫 5183-4757,异狄氏剂标准样品降解率最低,但在连续进样 10 次后,降解率不再满足标准规定的仪器性能检查要求.
Exploring the Factors Affecting the Degradation of Endrin in Gas Chromatography
Endrin is one of the common organochlorine pesticides.In this paper,gas chromatography(GC-ECD)was used to investigate the factors affecting the degradation of endrin.It was determined that in the pulse non split injection mode,when the injection port temperature was 280℃,the preferred choice was the ultra-high inert glass fiber liner 5190-2293 and non adhesive loss and temperature optimized BTO spacer 5183-4757.The degradation rate of the standard sample of endrin was the lowest,but after 10 consecutive injections,the degradation rate no longer met the instrument performance inspection requirements specified in the standard.

endringas chromatographyorganochlorine pesticides

徐欢、王景

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渭南市环境保护监测站,陕西 渭南 714000

异狄氏剂 气相色谱 有机氯农药

2024

山西化工
山西省煤化工发展促进中心 山西省化工学会

山西化工

影响因子:0.293
ISSN:1004-7050
年,卷(期):2024.44(10)