山西化工2024,Vol.44Issue(10) :89-90,104.DOI:10.16525/j.cnki.cn14-1109/tq.2024.10.029

紫外分光光度法和离子色谱法测定水中硝酸盐氮的比对分析

Comparative Analysis and Determination of Nitrate Nitrogen in Water by Ultraviolet Spectroscopy and Ion Chromatography

苗俊
山西化工2024,Vol.44Issue(10) :89-90,104.DOI:10.16525/j.cnki.cn14-1109/tq.2024.10.029

紫外分光光度法和离子色谱法测定水中硝酸盐氮的比对分析

Comparative Analysis and Determination of Nitrate Nitrogen in Water by Ultraviolet Spectroscopy and Ion Chromatography

苗俊1
扫码查看

作者信息

  • 1. 朔州市生态环境局平鲁分局,山西 朔州 036800
  • 折叠

摘要

本文通过紫外分光光度法和离子色谱法测定水中硝酸盐氮的含量,分别就取样量、检测时间、标准曲线、精密度、准确度等参数进行比对分析.结果显示,离子色谱法较紫外分光光度法所需的试样量少,而紫外分光光度法较离子色谱法分析时间短;同时,离子色谱法可同时测定多种无机阴离子;两种方法的标准曲线相关系数均大于0.999,回归方程均具有良好的线性关系;相对标准偏差分别为 1.6%、0.5%,加标回收率分别为 92.0%~102%、94.0%~110%,均满足质控要求.

Abstract

This article uses UV spectrophotometry and ion chromatography to determine the content of nitrate nitrogen in water,and compares and analyzes parameters such as sampling amount,detection time,standard curve,precision,and accuracy.The results showed that ion chromatography requires less sample size than ultraviolet spectrophotometry,while ultraviolet spectrophotometry has a shorter analysis time than ion chromatography;Meanwhile,ion chromatography can simultaneously measure multiple inorganic anions.The correlation coefficients of the standard curves for both methods are greater than 0.999,and the regression equations have a good linear relationship.The relative standard deviations are 1.6%and 0.5%,respectively,and the spiked recovery rates are 92.0%~102%and 94.0%~110%,respectively,all of which meet the quality control requirements.

关键词

硝酸盐氮/水质监测/紫外分光光度法/离子色谱法

Key words

nitrate nitrogen/water quality monitoring/ultraviolet spectroscopy/ion chromatography

引用本文复制引用

出版年

2024
山西化工
山西省煤化工发展促进中心 山西省化工学会

山西化工

影响因子:0.293
ISSN:1004-7050
段落导航相关论文