上海计量测试2024,Vol.51Issue(4) :11-13,17.

二氧化硅抛光液中金属杂质的检测方法

Method for detection of metal impurities in silica slurry

郝萍
上海计量测试2024,Vol.51Issue(4) :11-13,17.

二氧化硅抛光液中金属杂质的检测方法

Method for detection of metal impurities in silica slurry

郝萍1
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作者信息

  • 1. 上海市计量测试技术研究院
  • 折叠

摘要

采用高分辨电感耦合等离子质谱仪检测二氧化硅抛光液中金属杂质元素,通过调节元素分辨力,选择适合的同位素进行检测,可有效解决质谱干扰问题.采用标准加入法稀释样品检测金属杂质含量的方法,10 μg/kg加标回收率为81.17%~111.79%,可以实现对二氧化硅抛光液中多金属杂质的快速分析.

Abstract

In this paper,the high resolution inductively coupled plasma mass spectrometeris used to detect metal impurities in silicon oxide polishing liquid.By adjusting element resolution and selecting suitable isotope for detection,the problem of mass spectrum interference can be effectively solved.The standard addition method was used to dilute the samples for the detection of metal impurities,and the recovery rate of 10 μg/kg was between 81.17%and 111.79%,which can realize the rapid analysis of metal impurities in silica slurry.

关键词

高分辨电感耦合等离子体质谱仪/金属杂质/标准加入法/二氧化硅抛光液

Key words

HR-ICP-MS/trace metalimpurities/standard addition method/silica slurry

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出版年

2024
上海计量测试
上海市计量测试技术研究院,上海市计量测试学会,上海市计量协会

上海计量测试

影响因子:0.171
ISSN:1673-2235
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