世界农药2024,Vol.46Issue(9) :52-56.DOI:10.16201/j.cnki.cn10-1660/tq.2024.09.10

375g/L联苯菊酯·溴氰虫酰胺OD的高效液相色谱测定

Determination of bifenthrin·cyantraniliprole 375 g/L OD by HPLC

龚国华
世界农药2024,Vol.46Issue(9) :52-56.DOI:10.16201/j.cnki.cn10-1660/tq.2024.09.10

375g/L联苯菊酯·溴氰虫酰胺OD的高效液相色谱测定

Determination of bifenthrin·cyantraniliprole 375 g/L OD by HPLC

龚国华1
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作者信息

  • 1. 浙江省龙游东方阿纳萨克作物科技有限公司,浙江 衢州 324000;衢州市浙工大生态工业创新研究院,浙江 衢州 324400
  • 折叠

摘要

建立了一种可用于测定375 g/L联苯菊酯·溴氰虫酰胺可分散油悬浮剂(OD)中有效成分的高效液相色谱分析方法.采用岛津Inertsil ODS-3 C18柱为固定相,以甲醇+水溶液为流动相,在230 nm的检测波长下,对375 g/L联苯菊酯·溴氰虫酰胺OD试样中联苯菊酯和溴氰虫酰胺进行分离和分析.研究结果表明,在该色谱检测方法下,联苯菌酯和溴氰虫酰胺的线性相关系数均为 0.9999,标准偏差分别为0.0957和 0.0843,变异系数分别为0.50%和0.52%,平均回收率分别为 99.35%和 99.48%.说明该方法具有线性相关性好、精密度和准确度高等特点,可用于溴氰虫酰胺·联苯菊酯OD产品的质量分析检测.

Abstract

A high performance liquid chromatography(HPLC)analytical method was established for the determination of active ingredients in bifenthrin·cyantraniliprole 375 g/L oil dispersion(OD).The separation and quantitative analysis of bifenthrin·cyantraniliprole 375 g/L OD by HPLC were conducted by UV detector at 230 nm with methanol and water as mobile phase,and ODS-3 C18 column as fixed phase.The results showed that the linear correlation coefficient for both bifenthrin and cyantraniliprole were 0.9999,with standard deviations of 0.0957 and 0.0843,respectively,coefficients of variation of 0.50%and 0.52%,respectively,and average recoveries of 99.35%and 99.48%.This indicates that the method has good linear correlation,high precision and accuracy,and can be used for the quality analysis and detection of bifenthrin·cyantraniliprole OD.

关键词

联苯菊酯/溴氰虫酰胺/可分散油悬浮剂/高效液相色谱/分析

Key words

bifenthrin/cyantraniliprole/OD/HPLC/analysis

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出版年

2024
世界农药
上海市农药研究所

世界农药

影响因子:0.494
ISSN:1009-6485
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