塑料2024,Vol.53Issue(6) :6-10.

增韧聚乳酸3D打印材料的制备及力学性能

Preparation and Mechanical Properties of Toughened Poly(Lactic Acid)3D Printing Feedstock

彭茂荣 肖湘莲 钟一鸣 刘云馨 贺凌锋 赵婷 游琳 谢艳萍 阳博文
塑料2024,Vol.53Issue(6) :6-10.

增韧聚乳酸3D打印材料的制备及力学性能

Preparation and Mechanical Properties of Toughened Poly(Lactic Acid)3D Printing Feedstock

彭茂荣 1肖湘莲 2钟一鸣 1刘云馨 1贺凌锋 1赵婷 1游琳 1谢艳萍 1阳博文1
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作者信息

  • 1. 湖南工学院,材料科学与工程学院,湖南,衡阳 421002
  • 2. 湖南工学院,材料科学与工程学院,湖南,衡阳 421002;衡山县佳诚新材料有限公司,湖南,衡阳 421342
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摘要

以聚乳酸(PLA)为原材料,以抗冲改性剂BPM520为增韧剂,通过熔融共混法制备了增韧PLA 3D打印材料.研究了增韧改性对PLA的力学性能、熔体流动速率、复数黏度和热性能的影响,并且,采用5因素4水平正交试验对增韧PLA线材的3D打印工艺参数进行研究,得到最佳工艺参数.结果表明,与PLA原料相比,增韧PLA材料的韧性提高,断裂伸长率由11.8%提高至33.8%,冲击强度由29.1 J/m增大至70.7 J/m;增韧PLA材料的加工性能提高;通过正交试验结果分析获得增韧PLA线材最佳3D打印工艺参数为层高为0.25 mm、填充率为100%、壁厚为1.2 mm、打印速度为60 mm/s,填充图案为直线.在最佳工艺条件下,3D打印制得的增韧PLA样条表现出比参比PLA样条更高的拉伸性能和冲击强度.

Abstract

Toughened poly(lactic acid)(PLA)3D printing feedstock was prepared via melt-compounding using PLA as raw materials and impact modifier BPM520 as toughening agent.The effect of toughening on the mechanical properties,melt flow rate,complex viscosity and thermal properties of PLA was investigated.The five-factor and four-level design of orthogonal experiment was conducted to obtain the optimal 3D printing process parameters of modified PLA.The results indicated that toughened PLA showed improved toughness,the elongation at break increased from 11.8%to 33.8%,the impact strength increased from 29.1 J/m to 70.7 J/m with respect to pure PLA.The modified PLA also showed higher processability.The optimal 3D printing process parameters of toughened PLA obtained from orthogonal experimental results analysis were proposed as layer height 0.25 mm,infill density 100%,wall thickness 1.2 mm,print speed 60 mm/s,and infill pattern lines.The 3D-printed test samples from toughened PLA prepared at the optimal process parameters exhibited higher tensile properties and impact strength than the samples 3D-printed from reference PLA filament.

关键词

聚乳酸/增韧/3D打印/工艺参数/力学性能/正交试验

Key words

poly(lactic acid)/toughening/3D printing/process parameters/mechanical properties/orthogonal experiment

引用本文复制引用

出版年

2024
塑料
北京市塑料研究所

塑料

CSTPCDCSCD北大核心
影响因子:1.163
ISSN:1001-9456
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