首页|气相色谱法同时测定包装用塑料复合膜袋中13种有机溶剂残留量

气相色谱法同时测定包装用塑料复合膜袋中13种有机溶剂残留量

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采用气相色谱法建立一种测定包装用塑料复合膜袋中13种有机溶剂残留量的分析检测方法.方法选用Rtx-5石英毛细管柱(50m×0.32 mm,0.5 μm)和氢火焰离子化检测器FID,13种有机溶剂在15 min内分离良好.该方法在0.03~0.6 mg/m2(3-甲基戊烷范围为0.015~0.3 mg/m2)范围内线性关系良好,13种目标物的相关系数均大于0.998,检出限范围为0.001~0.005 mg/m2,7次测定相对标准偏差在1.04%~7.55%,样品加标回收率范围为95.4%~114.2%.测定了 6种塑料包装材料中的有机溶剂残留量,方法快速、准确、再现性好,完全能满足塑料复合膜袋中13种溶剂残留量的测定.
Simultaneous determination of 13 kinds of organic solvent residues in plastic laminated films and pouches for packaging by gas chromatography
An analytical method for the determination of 13 kinds of organic solvent residues in plastic laminated films and pouches for packaging by gas chromatography was established.The Rtx-5 capillary column(50 m×0.32 mm,0.5 μm)and hydrogen flame ionization detector were selected,13 kinds of organic solvents were separated from each other well within 15 min.The method has the good linearity in the range of 0.03~0.6 mg/m2(3-methylpentane is in the range of 0.015~0.3 mg/m2)(r>0.998),the limits of detection are 0.001~0.005 mg/m2,RSD(n=7)are in the range of 1.04%~7.55%and the recoveries are 95.4%~110.1%.During the experiments,the organic solvent residues in 6 kinds of plastic packaging materials were analyzed.This is a fast and accurate way with good reproducibility and can fully meet the determining of 13 kinds of organic solvent residues in plastic laminated films and pouches for packaging.

gas chromatographyorganic solvent residueplastic packing material

刘宁宁

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康达新材料(集团)股份有限公司,上海 201419

气相色谱 有机溶剂残留 塑料包装材料

2024

塑料包装
中轻投资有限公司

塑料包装

影响因子:0.1
ISSN:1006-9828
年,卷(期):2024.34(1)
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