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胶黏剂黏度测试方法的比较

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黏度是胶黏剂的一项重要性能指标.本文研究了不同测试方法对牛顿流体型胶黏剂(聚氨酯类和环氧类胶黏剂)、溶剂挥发型胶黏剂(溶剂型苯乙烯-丁二烯-苯乙烯嵌段共聚物和聚氨酯类胶黏剂)、热熔型胶黏剂(乙烯-醋酸乙烯酯共聚物、聚烯烃、聚酰胺)的黏度的影响,研究了采用不同的测试方法、同一方法不同设备对牛顿流体型的环氧胶黏剂的黏度的影响.结果表明,对于牛顿流体型胶黏剂,采用单圆筒旋转黏度计法和旋转流变仪法的测试结果差异不大.对于溶剂挥发型胶黏剂,单圆筒旋转黏度计的测试结果具有较好的平行性.对于热熔型胶黏剂,锥板旋转黏度计和旋转流变仪的测试结果具有较好的一致性.该研究可为黏度的日常检测活动中的测试方法和条件的选择提供参考,也可为相关的质量控制活动的开展提供借鉴.
Comparisons of the Test Methods for Adhesive Viscosity
Viscosity is an important property of adhesives.This article investigated the effects of different testing methods on the viscosity of Newtonian-fluid adhesives(polyurethane and epoxy adhesives),solvent-volatile adhesives(solvent-based styrene butadiene styrene block copolymer and polyurethane adhesives),and hot-melt adhesives(ethylene-vinyl acetate copolymer,polyolefin,polyamide).The effects of different testing methods and different equipment using the same method on the viscosity of Newtonian-fluid epoxy adhesives were also investigated.The results show that,for the Newtonian-fluid adhesives,the result differences between the single cylinder rotating viscometer method and the rotating rheometer method are small.For solvent-volatile adhesives,the single cylinder rotary viscometer method has good parallelism.For hot-melt adhesives,the results of cone-plate viscometer and rheometer are consistent.This study could provide references for the selections of testing methods and conditions in daily viscosity tests,as well as for the developments of related quality control activities.

AdhesiveViscosityRotational RheometerRotary Viscometer

苏志明、李云华

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中国合格评定国家认可中心,北京 100062

康达新材料(集团)股份有限公司,上海 201419

胶黏剂 黏度 旋转流变仪 旋转黏度计

国家市场监督管理总局技术保障专项项目

2023YJ39

2024

塑料工业
中蓝晨光化工研究院有限公司

塑料工业

CSTPCD北大核心
影响因子:0.685
ISSN:1005-5770
年,卷(期):2024.52(9)
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