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盐析效应萃取生物柴油

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生物柴油是解决能源和环境问题的主要替代燃油之一.研究了一种利用盐析效应萃取生物柴油的方法,结果表明,硫酸钠的效果最好.在单因素实验的基础上,进行了二次回归正交实验,建立了回归方程数学模型,最佳萃取条件为:硫酸钠溶液浓度5.49 mol/L,萃取时间37 min,此时预测的生物柴油得率为97.99%,实测的生物柴油得率为97.957%,实验结果与模型预测值相近,说明采用二次多项式回归分析得到的提取条件可用.
Salting-out effect on extraction of biodiesel
Biodiesel is one of the main substitute fuel to solve the problem of environment and energy. Salting-out extraction was used for recover)' of biodiesel, the results showed that the effect of sodium sulfate was the best. On the Hasis of single-factor experiment, second regression of central composite design, and establish to a mathematical models of regression equation, the optimal extraction conditions were as follows; sodium sulfate solution 5. 49 mol/L, extraction time 37 min, the predicted biodiesel rate was 97.99% ,the experimental value was 97.957% ,which was agreed with model predictions,the conditions obtained by regression analysis of central composite were applicable.

crude biodieselsalting-outextraction

龚旌

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闽江学院化学与化学工程系,福建福州350108

粗生物柴油 盐析 萃取

福建省科技计划项目

2007C0006

2012

应用化工
陕西省石油化工研究设计院 陕西省化工学会

应用化工

CSTPCDCSCD
影响因子:0.411
ISSN:1671-3206
年,卷(期):2012.41(12)
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