应用化工2024,Vol.53Issue(8) :1853-1858.

1,2-茚二酮显现纸张表面汗潜指印及配方优化研究

Development of sweat latent fingermarks and formulation optimization of 1,2-indandione on paper

梁帅 高树辉 邓人彬
应用化工2024,Vol.53Issue(8) :1853-1858.

1,2-茚二酮显现纸张表面汗潜指印及配方优化研究

Development of sweat latent fingermarks and formulation optimization of 1,2-indandione on paper

梁帅 1高树辉 2邓人彬3
扫码查看

作者信息

  • 1. 中国人民公安大学 侦查学院,北京 100038;天津公安警官职业学院,天津 300000
  • 2. 中国人民公安大学 侦查学院,北京 100038
  • 3. 重庆铁路公安处,重庆 401100
  • 折叠

摘要

基于激光检验照相及控制变量法,对茚二酮显现配方进行优化,研究添加冰醋酸、氯盐对指印显现效果的影响.结果表明,最优配方为:0.25 g茚二酮、225 mL乙酸乙酯、225 mL石油醚、25 mL冰醋酸、25 mL储存液(0.2 g氯化锌、30 mL乙醇),且适用于国内的气候环境,对渗透性客体表面新鲜及20d以内较陈旧指印均具有较好的显现效果,指印荧光显著增强,实现对渗透性客体上汗潜指印的比色与荧光双模式显现,但应注意渗透性客体特性、冰醋酸用量及氯盐种类.

Abstract

Based on laser inspection photography and control variable method,the development formula of indandione was systematically studied,the formulations were optimised,the influence of adding glacial acetic acid and chlorine salt to the formula on the development effect of fingermarks was further studied.The results showed that the optimal formula was formula:0.25 g indandione,225 mL ethyl acetate,225 mL petroleum ether,25 mL ice acetic acid,25 mL storage solution(0.2 g zinc chloride,30 mL etha-nol),and suitable for domestic climate environment,which had a good effect on the porous objects of fresh and within 20 d of the aged left fingermarks;fingermark fluorescence was significantly enhanced.The ex-perimental results provide a method to follow for optimizing the formulation of indandione fingerprint de-velopment,realizing the colorimetric and fluorescence dual-mode development of sweat latent fingermarks on porous objects.But attention should be paid to the characteristics of the porous object and the control of the amount of glacial acetic acid and the type of chlorine salt.

关键词

茚二酮/汗潜指印/比色/荧光/优化配方

Key words

indanedione/latent sweat fingermarks/colorimetric/fluorescence/optimal formulation

引用本文复制引用

基金项目

公安科技成果推广引导计划项目(2023-24)

中国人民公安大学刑事科学技术双一流创新研究专项(2023SYL06)

出版年

2024
应用化工
陕西省石油化工研究设计院 陕西省化工学会

应用化工

CSTPCD北大核心
影响因子:0.411
ISSN:1671-3206
段落导航相关论文