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电子束辐照对酸枣仁中黄曲霉毒素及斯皮诺素含量的影响

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为明确电子束辐照对酸枣仁中黄曲霉毒素(AFB1、AFB2、AFG1、AFG2)的降解效果及斯皮诺素的影响。利用高效液相色谱法研究不同辐照剂量、不同含水量对酸枣仁中黄曲霉毒素(AFB1、AFB2、AFG1、AFG2)及斯皮诺素含量的影响。结果表明,乙腈溶液中AFB1、AFB2、AFG1、AFG2 的降解率随辐照剂量的增加呈上升趋势;8 kGy 辐照处理的AFB1、AFB2、AFG1、AFG2 降解率最高,分别为97。25%、93。59%、75。11%、69。70%。随着辐照剂量和含水量的增加,酸枣仁中黄曲霉毒素的降解率呈上升趋势。含水量为23%的酸枣仁处理后黄曲霉毒素的降解率分别为 30。58%、30。24%、38。04%、36。58%;经不同辐照剂量处理后的斯皮诺素的含量变化差异不显著(P>0。05),含水量为7%酸枣仁辐照处理后斯皮诺素的含量显著高于15%、19%、23%含水量的酸枣仁。因此,电子束辐照结合水分处理能有效降解酸枣仁中的黄曲霉毒素,然而水分含量过高不利于斯皮诺素含量的保持。
Effects of Electron Beam Irradiation on Contents of Aflatoxin and Spinosin in Ziziphi Spinosae Semen
This study aimed to determine the effect of electron beam irradiation on the degradation of afla-toxins(AFB1,AFB2,AFG1,AFG2)and spinosin in Ziziphi Spinosae Semen.The effects of different irradiation doses and different water contents on the contents of aflatoxins(AFB1,AFB2,AFG1,AFG2)and spinosin in Ziziphi Spinosae Semen were investigated using high-performance liquid chromatography.The results showed that the degradation rates of AFB1,AFB2,AFG1,and AFG2 treated with acetonitrile solution increased with irra-diation dose,and the degradation rates of AFB1,AFB2,AFG1,and AFG2 treated with 8 kGy irradiation were 97.25%,93.59%,75.11%,and 69.70%,respectively.With the increase of irradiation dose and water con-tent,the degradation rate of aflatoxin in Ziziphi Spinosae Semen also increased.The aflatoxin degradation rates of Ziziphi Spinosae Semen with 23%water content were 30.58%,30.24%,38.04%,and 36.58%,respectively.There was no significant difference in the content of spinosin after different irradiation doses(P>0.05).The content of spinosin in Ziziphi Spinosae Semen irradiated with 7%water content was significantly higher than that in Ziziphi Spinosae Semen with water contents of 15%,19%,and 23%.In conclusion,electron beam irradia-tion combined with water treatment can effectively degrade aflatoxin in Ziziphi Spinosae Semen;however,too high water content is not conducive to the maintenance of spinosin content.

Ziziphi Spinosae SemenAflatoxin flasvusElectron beam irradiationSpinosin

马力辉、李迅、庞艳苹、高原、崔炎、赵志磊

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河北大学 质量技术监督学院,河北 保定 071002

计量仪器与系统国家地方联合工程研究中心,河北 保定 071002

河北省能源计量与安全检测技术重点实验室,河北 保定 071002

保定市市场监督管理局食品执法支队食品药品检验所,河北 保定 071002

河北大学地理标志研究院,河北 保定 071002

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酸枣仁 黄曲霉毒素 电子束辐照 斯皮诺素

河北省重点研发计划项目课题

21344801D

2024

陕西农业科学
西北农林科技大学

陕西农业科学

CSTPCD
影响因子:0.388
ISSN:0488-5368
年,卷(期):2024.70(8)