首页|液相色谱在柴油多环芳烃分析中的应用

液相色谱在柴油多环芳烃分析中的应用

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本文旨在应用高效液相色谱(HPLC)技术对柴油中的多环芳烃(PAHs)进行定性和定量分析.PAHs是一类具有高毒性和致癌性的有机化合物,对环境和人体健康构成严重威胁.实验中,通过液液萃取法提取柴油样品中的PAHs,使用氰基键合硅胶固定相进行色谱分析.结果表明,所采用的HPLC方法能够有效分离和检测柴油中的多种PAHs,具有较高的分辨率和灵敏度.主要检测的PAHs包括双环芳烃(DAHs)和三环芳烃(T+AHs).实验结果显示,不同PAHs在柴油中的浓度分布反映了其燃烧特性和污染来源.该方法的有效性和可靠性在实验中得到了验证,但样品前处理和色谱条件的优化仍有改进空间.本文的研究为柴油中PAHs的分析提供了一个有效的技术手段,对环境监测和污染控制具有重要意义.
Application of liquid chromatography in the analysis of polycyclic aromatic hydrocarbons in diesel
This article aims to apply high-performance liquid chromatography(HPLC)technology for the qualitative and quantitative analysis of polycyclic aromatic hydrocarbons(PAHs)in diesel fuel.PAHs are a class of organic compounds with high toxicity and car-cinogenicity,posing serious threats to the environment and human health.In the experiment,PAHs in diesel samples were extracted using liquid-liquid extraction and analyzed chro-matographically using a cyanopropyl-bonded silica gel stationary phase.The results show that the adopted HPLC method can effectively separate and detect various PAHs in diesel,exhibiting high resolution and sensitivity.The primary PAHs detected include bicyclic aro-matic hydrocarbons(DAHs)and tricyclic aromatic hydrocarbons(T+AHs).The experimen-tal results indicate that the concentration distribution of different PAHs in diesel reflects their combustion characteristics and pollution sources.The effectiveness and reliability of this method were validated in the experiment,although there is still room for improvement in sample pretreatment and chromatographic conditions.This study provides an effective tech-nical means for the analysis of PAHs in diesel,which is of great significance for environ-mental monitoring and pollution control.

dieselliquid chromatographypolycyclic aromatic hydrocarbonsanalytical meth-odsenvironmental pollution

丁漪、李红、王芳

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中国石油宁夏石化公司,宁夏银川 750026

柴油 液相色谱 多环芳烃 分析方法 环境污染

2024

石油化工应用
宁夏化工学会

石油化工应用

影响因子:0.276
ISSN:1673-5285
年,卷(期):2024.43(9)