首页|生活饮用水中重金属铅检测方法研究

生活饮用水中重金属铅检测方法研究

Study on detection method of heavy metal lead in drinking water

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目的 优化准确、灵敏且实用的生活饮用水中重金属铅的检测方法,为饮用水安全监测提供有力的技术支持.方法 采用石墨炉原子吸收实验检测方法进行研究.对生活饮用水样本进行预处理,去除杂质和干扰物质,之后检测铅含量.实验过程中,通过优化实验条件、选择合适的试剂和仪器参数,以提高检测方法的灵敏度和准确性.结果 实验中测得铅的标准曲线具有良好的线性关系,线性系数大于 0.999.在设定的线性范围内,相对偏差较小,精密度较高.实验中进行了加标回收实验,测得加标回收率在 95%~105%之间,说明实验方法的准确性较高.实验中设定的灰化温度为 800℃,原子化温度为 1800℃.这些温度参数的设定有助于提高测量的灵敏度和准确性.浓度 0,5.00,10.00,20.00,30.00 μg/L以及标准样本测得的重金属铅吸光度分别是 0.0055、0.0468、0.0881、0.1532、0.2328.结论 石墨炉原子吸收实验检测方法属于生活饮用水中重金属铅检测的有效方法.该方法具有较高的灵敏度和准确性,能够满足饮用水安全监测的需求.通过应用该方法,可以有效地监测和控制生活饮用水中重金属铅的含量,保障人们的饮水安全.同时,该方法也为其他重金属元素的检测提供了有益的参考和借鉴.
Objective To optimize an accurate,sensitive and practical method for detecting heavy metal lead in drinking water,and to provide strong technical support for drinking water safety monitoring.Methods The graphite furnace atomic absorption test was used for the study.Samples of drinking water are pretreated to remove impurities and disturbing substances and then tested for lead levels.In the process of experiment,the sensitivity and accuracy of the detection method were improved by optimizing the experimental conditions,selecting the appropriate reagents and instrument parameters.Results The standard curve of lead measured in the experiment has a good linear relationship,and the linear coefficient is greater than 0.999.Within the set linear range,the relative deviation is small and the precision is high.The recovery rate is 95%~105%,indicating the accuracy of the experimental method.The ashing temperature set in the experiment is 800℃,and the atomization temperature is 1800℃.The setting of these temperature parameters helps to improve the sensitivity and accuracy of the measurement.Concentrations of 0,5.00,10.00,20.00,30.00 μg/L and standard samples were 0.0055,0.0468,0.0881,0.1532 and 0.2328,respectively.Conclusion Graphite furnace atomic absorption assay is an effective method for detecting heavy metal lead in drinking water.The method has high sensitivity and accuracy,and can meet the needs of drinking water safety monitoring.By using this method,the content of heavy metal lead in drinking water can be monitored and controlled effectively,and the drinking water safety can be guaranteed.At the same time,this method also provides a useful reference for the detection of other heavy metal elements.

drinking waterheavy metal leaddetection method

管琛

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淄博市临淄区疾病预防控制中心,淄博 255000

生活饮用水 重金属铅 检测方法

2024

实验室检验
中国检验检测学会

实验室检验

ISSN:2097-261X
年,卷(期):2024.2(4)
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