首页|凝胶色谱法测定聚丙烯二甲苯可溶物含量

凝胶色谱法测定聚丙烯二甲苯可溶物含量

Determination content of xylene soluble matter in polypropylene by gel chromatography

扫码查看
目的 本研究旨在探究凝胶色谱法在测定聚丙烯二甲苯中可溶物含量中的应用.方法 研究采用凝胶色谱法对聚丙烯中二甲苯可溶物含量进行了精确测定,并与容量法进行对比分析,验证了凝胶色谱法的准确性和可靠性.结果 实验结果显示,凝胶色谱法测定结果与容量法相比,测试绝对差值不超过 0.07%,符合准确度要求.此外,凝胶色谱法显著缩短了分析时间,从容量法的约 8 小时缩短至 3 小时,且操作更为简便,样品处理过程中二甲苯用量大幅减少,体现了其高效与环保性.结论 本研究成功验证了凝胶色谱法在聚丙烯中二甲苯可溶物含量测定中的可行性和优越性.该方法不仅操作简便、分析速度快,而且环保性强,对环境和操作人员的影响小,为聚丙烯产品质量的快速检测与控制提供了有力支持,具有广泛的工业应用前景.
Objective This study aims to explore the application of gel permeation chromatography in determining the content of xylene-soluble substances in polypropylene.Methods The study employed gel chromatography to accurately measure the content of xylene-soluble substances in polypropylene and conducted a comparative analysis with the volumetric method to verify the accuracy and reliability of gel chromatography.Results The experimental results indicated that the absolute difference between the measurement results obtained by gel chromatography and the volumetric method did not exceed 0.07%,meeting the accuracy requirements.Furthermore,gel chromatography significantly shortened the analysis time from approximately 8 hours with the volumetric method to 3 hours,and the operation was more straightforward.The amount of xylene used during sample processing was greatly reduced,demonstrating its efficiency and environmental friendliness.Conclusion This study successfully validated the feasibility and superiority of gel chromatography in determining the content of xylene-soluble substances in polypropylene.This method is not only simple to operate and fast in analysis but also highly environmentally friendly,with minimal impact on the environment and operators.It provides strong support for the rapid detection and control of polypropylene product quality and holds broad industrial application prospects.

polypropylene powdergel chromatographyvolumetric method

赵芳、李尚滨

展开 >

国能包头化工有限责任公司,包头 014010

聚丙烯粉料 凝胶色谱仪 容量法

2024

实验室检验
中国检验检测学会

实验室检验

ISSN:2097-261X
年,卷(期):2024.2(12)