首页|量子点纳滤膜制备及染料去除性能实验教学设计

量子点纳滤膜制备及染料去除性能实验教学设计

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将膜分离实验与科学研究有机融合,设计了量子点复合纳滤膜制备及染料去除性能研究性实验.通过低温固相法合成氮化碳量子点,并以其为水相单体制备量子点复合纳滤膜.利用红外光谱、扫描电镜等对膜结构和形貌进行表征分析.氮化碳量子点与异氰酸酯发生反应,形成致密无缺陷的聚脲分离层.染料去除性能测试表明,制备的量子点纳滤膜可以有效去除水中的刚果红、甲基蓝、溴百里酚蓝钠盐、甲基红等负电性染料;随着氮化碳量子点浓度增加,复合纳滤膜水通量逐渐增大,甲基蓝去除率则呈现先升高后降低的趋势.实验涵盖了文献调研、材料制备、结构表征和性能测试,可使学生掌握多种实验技能,充分激发创新潜能,从而提高学生的自主学习能力、科学探究能力和创新实践能力.
Experimental Teaching Design on Preparation and Dye Removal Performance of Quantum Dot Nanofiltration Membranes
Guided by the training of innovative talents,the research experiments about the preparation of quantum dot composite nanofiltration membranes and their dye removal performance are designed through the integration of membrane separation experiments and scientific research.Carbon nitride quantum dots are synthesized by low-temperature solid-phase method,and used as aqueous monomers to fabricate quantum dot composite nanofiltration membranes.Infrared spectroscopy and scanning electron microscopy are used to characterize and analyze the structure and morphology of the membranes.Carbon nitride quantum dots are reacted with isocyanates to form a dense and defect-free polyurea separation layer.The dye removal performance test shows that the prepared quantum dot nanofiltration membrane can effectively remove negative electric dyes such as congo red,methyl blue,bromothymol blue sodium salt and methyl red in water.With the increase of carbon nitride quantum dot concentration,the water flux of composite nanofiltration membrane gradually increases,and the methyl blue removal rate shows a trend of first increasing and then decreasing.The experiment covers literature research,material preparation,structural characterization and performance testing,which can enable students to master a variety of experimental skills and fully stimulate their innovation potential,thereby improving students'independent learning ability,scientific inquiry ability and innovative practice ability.

quantum dotnanofiltration membranesdye removal performanceexperimental design

白云翔、陈鑫、董亮亮、张春芳

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江南大学合成与生物胶体教育部重点实验室化学与材料工程学院,江苏无锡 214122

量子点 纳滤膜 染料去除性能 实验设计

国家自然科学基金面上项目国家自然科学基金面上项目江南大学本科教育教学改革研究项目

2207510722278177JG2021132

2024

实验室研究与探索
上海交通大学

实验室研究与探索

CSTPCD北大核心
影响因子:1.69
ISSN:1006-7167
年,卷(期):2024.43(2)
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