实验室研究与探索2024,Vol.43Issue(2) :175-179.DOI:10.19927/j.cnki.syyt.2024.02.034

荧光碳点复合材料显现潜手印综合实验设计

Design of Comprehensive Experimental Teaching for Fluorescent Carbon Dots-based Composites in the Development of Latent Fingerprints

王稳 孙广婷 卫金保 孟利 左琦 朱倩倩
实验室研究与探索2024,Vol.43Issue(2) :175-179.DOI:10.19927/j.cnki.syyt.2024.02.034

荧光碳点复合材料显现潜手印综合实验设计

Design of Comprehensive Experimental Teaching for Fluorescent Carbon Dots-based Composites in the Development of Latent Fingerprints

王稳 1孙广婷 2卫金保 2孟利 1左琦 1朱倩倩2
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作者信息

  • 1. 河南警察学院刑事科学技术系,郑州 450046
  • 2. 郑州大学化学学院,郑州 450001
  • 折叠

摘要

为了提高学生的证据意识和综合科研能力,设计了一个涵盖碳点复合材料合成、结构表征和潜手印显现应用的综合性实验.以柠檬酸、三乙烯四胺和罗丹明6G为原料合成荧光碳点材料,通过自组装策略将碳点纳米颗粒原位嵌入金属有机骨架中,从而获得固态下具有强荧光发射的碳点复合材料.利用扫描电子显微镜、荧光光谱仪、粉末X射线衍射仪等分析仪器对复合材料进行表征.采用粉末刷显法将制备的复合材料用于不同客体表面的潜手印显现中,对显现效果进行了分析和评价.教学内容紧密联系学术前沿和实际应用,有助于提高学生分析问题、解决问题的能力,培养创新的科研精神.

Abstract

To improve students'evidence awareness and comprehensive scientific research ability,a carbon dots-based composite material is obtained with strong fluorescence emission in solid state.Based on this material,a comprehensive and innovative experiment covering the synthesis of fluorescent composites,characterization,and the development of latent fingerprints is designed.Citric acid,triethylenetetramine and rhodamine 6G are used as raw materials to synthesize fluorescent carbon dots.The prepared carbon dots are further embedded in metal-organic frameworks through a self-assembly strategy to give rise to a solid emissive composite material.The composite material is characterized by scanning electron microscope,fluorescence spectrometer,powder X-ray diffractometer and other instruments.The prepared composite material is applied to develop latent fingerprints on different substrates by a powder-dusting method,and the developing performance is further analyzed and evaluated.The experiment is highly comprehensive and innovative,and the teaching content is closely linked with the academic frontier and practical application,which is conducive to improve problem-analyzing and solving abilities,and cultivate innovative scientific research spirit of students.

关键词

碳量子点/金属有机骨架/潜手印显现/综合实验

Key words

carbon dots/metal organic framework/latent fingerprint development/comprehensive experiment

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基金项目

教育部人文社会科学研究青年基金(21YJC820056)

国家级大学生创新创业训练计划(202210459153)

河南省重点研发与推广专项(232102230002)

河南警察学院教学改革项目(SZ2021014)

出版年

2024
实验室研究与探索
上海交通大学

实验室研究与探索

CSTPCD北大核心
影响因子:1.69
ISSN:1006-7167
参考文献量16
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