首页|BaTiO3优化制备及压电催化性能分析的综合实验设计

BaTiO3优化制备及压电催化性能分析的综合实验设计

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为了实现前沿压电催化水污染控制技术、大型仪器分析技术与实践操作能力培养的有机结合,设计了一个综合水污染控制工程实验——BaTiO3优化制备及压电催化性能分析.通过对BaTiO3进行不同时间的热处理,有效优化BaTiO3压电催化降解染料性能.利用电子顺磁共振波谱仪(ESR)分析降解过程中自由基的生成,并借助猝灭实验明确不同自由基在染料降解过程中的作用.结果表明,对BaTiO3进行2 h热处理可有效提高其压电催化降解罗丹明B(RhB)染料的性能.ESR检测分析反应体系能产生羟基自由基、单线态氧和超氧自由基,而猝灭实验结果表明羟基自由基在染料降解过程中起主导作用.
Integrated Experiment Design for Optimized Preparation and Piezocatalysis Performance Analysis of BaTiO3
In order to organically combine the latest water treatment technique,large-scale instrument analysis and operation capability cultivation,a novel integrated experiment for the optimized preparation and piezocatalysis performance analysis of BaTiO3 is systematically designed.The piezocatalytic performance of BaTiO3 nanomaterial on the dye degradation is effectively optimized by heat treatment.The generation of free radicals during the degradation process is analyzed by electron spin resonance(ESR)technique,and the role of different radicals in the dye degradation is confirmed by quenching experiment.The results show that 2 hours heat treatment of BaTiO3 can effectively improve the performance of the piezoelectric catalytic degradation of RhB dyes.The hydroxyl radical,singlet oxygen and superoxide radical are detected by ESR during the degradation process.The quenching experiments results show that hydroxyl radical plays a leading role in the process of dye degradation.

piezocatalysiswater pollution control experimentintegrated experiment design

于玲、白航、陈瑜

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广东工业大学分析测试中心,广州 510006

压电催化 水污染控制实验 综合实验设计

广东省基础与应用基础研究基金

2021A1515110742

2024

实验室研究与探索
上海交通大学

实验室研究与探索

CSTPCD北大核心
影响因子:1.69
ISSN:1006-7167
年,卷(期):2024.43(3)
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