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不同原料类型的黄酒对白芍酒炙品质的影响

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目的 比较不同种类原料酿制而成的黄酒对白芍饮片炮制后内在质量的影响,为制定炮制辅料用酒质量标准提供实验依据。方法 采用Box-Behnken响应面试验设计方法考察白芍酒炙工艺中的炮制温度(A)、炮制时间(B)、黄酒用量(C)3个因素,以5种指标性成分没食子酸,儿茶精,氧化芍药苷、芍药内酯苷、芍药苷的含量综合评分作为评价指标,建立酒炙白芍的最佳工艺。在该工艺条件下,以不同原料类型的黄酒为辅料,得到6个批次酒白芍成品。采用主成分分析和聚类分析法对检测结果进行综合评价。结果 黍米黄酒组的饮片中没食子酸,儿茶素,氧化芍药苷,芍药苷含量均高于其他黄酒组,小米黄酒组中芍药内酯苷含量高于其他组。主成分分析综合评分结果为:黍米黄酒>薯干黄酒>糯米黄酒>小米黄酒>大米黄酒>红曲黄酒。酒白芍的最佳炮制工艺为炮制温度84。6779℃,炮制时间为9。5012 min,黄酒用量为9。639%。结论 不同种类辅料黄酒对酒白芍饮片内在质量产生不同影响,建议选用黍米黄酒作为酒炙白芍炮制辅料用酒,Box-Be-hnken响应面法优选酒白芍工艺切实可行,具有较强的实际意义,为酒白芍生产提供了科学依据。
Influence of different raw materials on the quality of wine white peony
Objective To compare effects of rice wine made from different raw materials on the internal quality of Paeoniae Radix Alba slices after the preparation process,and to provide experimental basis for establishing the quality standard of wine used as processing ac-cessories.Methods The three factors of processing temperature(A),processing time(B)and dosage of rice wine(C)were investiga-ted by using the Box Behnken response surface design method.The comprehensive score of 5 index components,gallic acid,catechin,oxypaeoniflorin,albiflorin and paeoniflorin,were used as the evaluation index.Establish the best process of preparing Paeoniae Radix Alba pieces with wine.Under this process condition,6 batches of Paeoniae Radix Alba pieces with wine were obtained with different types of yellow rice wine as auxiliary materials.Principal component analysis and cluster analysis were used to evaluate the detection re-sults.Results The contents of gallic acid,catechin,oxypaeoniflorin and paeoniflorin in the decoction pieces of broomcorn millet rice wine group were higher than those of other rice wine groups,and the content of albiflorin in foxtail millet rice wine group was higher than that of other groups.The results of principal component analysis were as follows:broomcorn millet rice wine>dried potato rice wine>glutinous rice wine>foxtail millet rice wine>rice wine>red yeast rice wine.The best processing technology of Paeoniae Radix Alba pieces with wine:the optimum processing temperature was 84.6779℃,the processing time was 9.5012 min,and the dosage of rice wine was 9.639%.Conclusion Different kinds of auxiliary rice wine have different effects on the intrinsic quality of Paeoniae Radix Alba slices.It is recommended to use broomcorn millet rice wine as the auxiliary wine for the preparation of wine Paeoniae Radix Alba pieces.The Box-Behnken response surface method is feasible and has strong practical significance,which provides a scientific basis for the pro-duction of wine Paeoniae Radix Alba pieces.

Wine Paeoniae Radix AlbaPrepared in piecesYellow rice wineAuxiliary materialsResponse surface meth-odPrincipal component analysisCluster analysis

夏晨皓、李圳、史佳一、潘罗星、赵清

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河北大学中医学院,河北保定 071000

酒白芍 饮片 黄酒 辅料 响应面法 主成分分析 聚类分析

2024

时珍国医国药
时珍国医国药杂志社

时珍国医国药

北大核心
影响因子:0.887
ISSN:1008-0805
年,卷(期):2024.35(15)